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网站主页CAS数据库列表 195-19-7更多图谱苯并- 3 ,4 -菲(195-19-7)红外图谱(IR1)

苯并- 3 ,4 -菲

产品名称 苯并- 3 ,4 -菲

CAS号195-19-7

分子式C18H12

分子量228.29

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  • Mass

    MS-NW-1267          
    benzo(c)phenanthrene
    C18H12              (Mass of molecular ion:    228)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       2.6
          44.0       1.1
          87.0       1.1
          88.0       1.1
          99.0       1.0
         100.0       3.1
         101.0       4.1
         112.0       4.7
         112.5       2.8
         113.0      14.2
         113.5       4.2
         114.0       4.1
         200.0       1.7
         224.0       4.9
         225.0       4.3
         226.0      26.9
         227.0      28.4
         228.0     100.0
         229.0      18.8
         230.0       1.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H12 16.3 mg : 0.5 ml CDCl3
    benzo(c)phenanthrene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.130 B 8.006 C 7.883 D 7.813 E 7.669 F 7.612 J(C,D)=8.5HZ.

         Hz     ppm     Int.
    

       3653.08   9.141    318
       3648.56   9.130     44
       3648.07   9.129     42
       3644.65   9.120    333
       3205.20   8.021    318
       3203.61   8.017    349
       3199.95   8.007     57
       3199.58   8.006     53
       3197.27   8.001    377
       3195.80   7.997    404
       3155.88   7.897    388
       3151.86   7.887     42
       3151.49   7.886     42
       3151.00   7.885     42
       3147.46   7.876    696
       3125.85   7.822   1000
       3121.95   7.812     68
       3120.73   7.809     52
       3117.31   7.801    603
       3113.16   7.790     42
       3074.83   7.694    151
       3073.24   7.690    178
       3067.99   7.677    268
       3066.41   7.673    405
       3064.82   7.669    219
       3061.52   7.661     49
       3059.45   7.656    286
       3057.86   7.652    293
       3054.32   7.643     42
       3049.68   7.631    315
       3048.46   7.628    382
       3045.78   7.622     62
       3044.92   7.619     54
       3042.85   7.614    223
       3041.75   7.612    436
       3040.65   7.609    388
       3034.91   7.594    198
       3033.81   7.592    205
    


  • 1H NMR 89.56 MHz
    C18 H12 0.025 g : 0.5 ml CDCl3
    benzo(c)phenanthrene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.127 B 8.005 C 7.883 D 7.808 E 7.67 F 7.61 THE SHIFT VALUES WERE OBTAINED AT 400MHZ. J(A,E)=8.42HZ. J(B,F)=7.9HZ. J(B,E)=1.5HZ. J(C,D)=8.5HZ. J(A,F)=1.1HZ.

         Hz     ppm     Int.
    

        821.00   9.168    124
        818.94   9.145     92
        818.38   9.138     91
        816.31   9.115     53
        815.56   9.107     72
        814.88   9.099     48
        813.06   9.079     96
        811.88   9.066    152
        720.00   8.040    129
        718.13   8.019    104
        715.63   7.991     95
        714.38   7.977    125
        713.25   7.964    144
        710.44   7.933    286
        707.19   7.897     51
        701.38   7.832    622
        699.25   7.808   1000
        695.00   7.761     47
        692.63   7.734     89
        690.69   7.713    125
        688.00   7.683    264
        685.63   7.656    405
        681.88   7.614    513
        678.19   7.573    288
        676.38   7.553    218
        671.44   7.498     52
    

in CDCl3



KBr disc



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