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MassMS-IW-9448 2,6-difluorobenzyl alcohol C7H6F2O (Mass of molecular ion: 144)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.5 27.0 1.0 28.0 3.1 29.0 7.5 30.0 2.1 31.0 13.1 37.0 2.6 38.0 3.2 39.0 4.8 45.0 1.8 49.0 2.0 50.0 9.2 51.0 9.0 52.0 1.7 56.0 2.2 57.0 9.5 61.0 3.6 62.0 6.2 63.0 17.2 63.5 1.1 64.0 1.7 68.0 5.3 69.0 5.3 70.0 4.6 70.5 1.0 71.5 6.2 72.0 1.3 73.0 1.2 74.0 5.6 75.0 35.5 76.0 4.2 77.0 8.9 79.0 1.0 80.0 1.3 81.0 5.7 83.0 1.3 87.0 1.4 88.0 3.4 92.0 1.6 93.0 3.4 94.0 6.2 95.0 62.1 96.0 20.9 97.0 12.9 98.0 1.0 99.0 1.5 101.0 10.5 103.0 1.1 105.0 2.4 107.0 6.6 108.0 1.2 112.0 1.2 113.0 10.1 114.0 11.6 115.0 42.5 116.0 4.8 123.0 76.6 124.0 21.2 125.0 11.2 126.0 5.6 127.0 55.7 128.0 4.8 141.0 10.4 142.0 1.5 143.0 75.4 144.0 100.0 145.0 7.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 F2 O 0.05 ml : 0.5 ml CDCl3 2,6-difluorobenzyl alcohol 
Assign. Shift(ppm)
A 7.227 B 6.861 C 4.711 D 3.04
Hz ppm Int.2903.56 7.266 131 2897.09 7.250 257 2895.14 7.245 232 2890.50 7.233 169 2888.67 7.229 472 2886.72 7.224 185 2882.08 7.212 227 2880.25 7.207 296 2873.66 7.191 145 2756.10 6.897 84 2754.39 6.893 111 2749.88 6.881 564 2746.09 6.872 142 2741.94 6.861 731 2737.55 6.850 137 2733.76 6.841 486 2729.00 6.829 80 2727.54 6.825 63 1882.93 4.712 1000 1215.58 3.042 158
in CDCl3
liquid film
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