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网站主页CAS数据库列表 18881-17-9更多图谱(S)-1,2,3,4-四氢异喹啉-3-基-甲醇(18881-17-9)质谱(MS)

(S)-1,2,3,4-四氢异喹啉-3-基-甲醇

产品名称 (S)-1,2,3,4-四氢异喹啉-3-基-甲醇

CAS号18881-17-9

分子式C10H13NO

分子量163.22

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  • Mass

    MS-KW-0531          
    (S)-1,2,3,4-tetrahydro-3-isoquinolinemethanol
    C10H13NO            (Mass of molecular ion:    163)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          27.0       1.0
          28.0       2.3
          39.0       1.9
          50.0       1.0
          51.0       3.0
          52.0       1.2
          63.0       1.4
          64.0       1.0
          64.5       1.2
          65.0       3.4
          65.5       3.9
          66.0       2.4
          77.0       6.4
          78.0       4.0
          79.0       2.0
          89.0       1.0
          91.0       2.3
         102.0       1.3
         103.0       6.7
         104.0      10.8
         105.0       7.3
         115.0       5.6
         116.0       1.7
         117.0       7.0
         118.0       1.1
         130.0      27.9
         131.0       4.8
         132.0     100.0
         133.0      10.7
         144.0       1.9
         162.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10H13NO 0.039 g : 0.5 ml CDCl3
    (S)-1,2,3,4-tetrahydro-3-isoquinolinemethanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.12 B *1 7.10 C 7.056 D 6.986 E 4.00 F *2 3.724 G 3.57 J *2 3.502 K 3.009 L *3 2.540 M *3 2.588 assigned by C-H COSY

         Hz     ppm     Int.
    

       2856.08   7.145     42
       2853.89   7.139     75
       2848.88   7.127    335
       2847.42   7.123    446
       2843.63   7.113    929
       2840.09   7.105    700
       2838.26   7.100    505
       2833.38   7.088    133
       2830.94   7.082     91
       2828.37   7.075     82
       2824.47   7.065    353
       2820.93   7.057    302
       2817.63   7.048    149
       2815.56   7.043    193
       2796.88   6.996    324
       2791.26   6.982    265
       2788.09   6.975    224
       1617.80   4.047     43
       1600.22   4.003   1000
       1583.99   3.963     51
       1496.71   3.744    289
       1492.92   3.735    308
       1485.60   3.717    373
       1481.94   3.707    364
       1426.64   3.569    700
       1408.45   3.524    383
       1400.88   3.505    412
       1397.47   3.496    317
       1389.90   3.477    328
       1216.44   3.043     81
       1211.92   3.032    114
       1208.26   3.023    135
       1205.69   3.016    162
       1202.15   3.008    164
       1201.05   3.005    164
       1198.13   2.997    155
       1194.46   2.988    123
       1189.95   2.977     85
       1070.20   2.677     89
       1065.56   2.666    110
       1053.72   2.636    331
       1049.08   2.625    296
       1043.22   2.610    273
       1032.48   2.583    225
       1026.98   2.569     85
       1016.24   2.542     80
    

in CDCl3



KBr disk



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