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MassMS-IW-8228 2-difluoromethoxy-1,1,1-trifluoroethane C3H3F5O (Mass of molecular ion: 150)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.6 29.0 12.6 31.0 13.1 32.0 1.8 33.0 22.7 44.0 1.0 47.0 1.0 49.0 1.4 50.0 1.3 51.0 93.5 52.0 1.3 61.0 2.0 63.0 3.7 64.0 2.4 69.0 7.2 80.0 2.5 81.0 92.4 82.0 2.4 83.0 100.0 84.0 2.3 131.0 8.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H3 F5 O 0.05 ml : 0.5 ml CDCl3 2-difluoromethoxy-1,1,1-trifluoroethane 
Assign. Shift(ppm)
A 6.304 B 4.182
Hz ppm Int.2591.67 6.485 239 2591.19 6.484 242 2519.65 6.305 469 2519.17 6.304 486 2447.63 6.125 239 2447.14 6.124 242 1683.96 4.214 322 1683.47 4.213 332 1675.78 4.194 879 1675.29 4.192 968 1667.60 4.173 900 1667.11 4.172 1000 1663.09 4.162 27 1662.48 4.160 27 1659.42 4.153 338 1658.94 4.151 349
in CDCl3
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