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MS2014-05010CW p-chlorophenethyl alcohol C8H9ClO (Mass of molecular ion: 156)
Source Temperature: 250 °C Sample Temperature: 200 °C Reservoir, 70 eV
28.0 15.0 31.0 1.7 32.0 3.7 39.0 2.4 50.0 1.8 51.0 2.6 62.0 1.6 63.0 5.5 64.0 1.1 65.0 2.7 73.0 1.7 74.0 1.1 75.0 2.3 77.0 2.8 89.0 14.9 90.0 4.9 91.0 28.6 92.0 2.3 99.0 5.1 101.0 2.1 102.0 1.4 103.0 2.0 112.0 1.1 125.0 100.0 126.0 25.8 127.0 33.0 128.0 8.2 138.0 1.7 156.0 30.7 157.0 2.8 158.0 9.9
90 MHz in CDCl3
in CDCl3
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1H NMR 89.56 MHz C8 H9 Cl O 0.05 ml : 0.5 ml CDCl3 p-chlorophenethyl alcohol Assign. Shift(ppm)
A *1 7.24 B *1 7.13 C 3.76 D 2.775 E 2.3
Hz ppm Int.
656.25 7.328 56 654.63 7.310 247 653.94 7.302 164 652.19 7.283 128 648.38 7.240 242 646.00 7.214 1000 644.25 7.194 301 641.88 7.168 287 640.50 7.152 811 637.81 7.122 186 634.00 7.080 119 631.56 7.052 201 627.13 7.003 25 348.63 3.893 27 254.56 2.843 338 248.00 2.770 562 244.00 2.725 47 241.44 2.696 239 205.63 2.297 103
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