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MassMS-NW-7289 tris(2-chloroethyl) orthoformate C7H13Cl3O3 (Mass of molecular ion: 250)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.1 27.0 18.3 28.0 2.7 29.0 2.6 31.0 11.1 43.0 2.3 45.0 6.7 47.0 4.7 49.0 2.7 51.0 1.0 62.0 4.8 63.0 100.0 64.0 3.8 65.0 33.0 73.0 40.4 74.0 1.5 109.0 7.6 111.0 2.8 137.0 1.3 171.0 56.4 172.0 3.5 173.0 36.8 174.0 2.3 175.0 6.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H13 Cl3 O3 0.05 ml : 0.5 ml CDCl3 tris(2-chloroethyl) orthoformate 
Assign. Shift(ppm)
A 5.371 B 3.874 C 3.687
Hz ppm Int.481.06 5.372 601 355.25 3.967 260 353.31 3.945 333 350.56 3.915 403 348.69 3.894 878 347.25 3.878 684 343.81 3.839 920 343.00 3.830 966 339.81 3.795 153 339.38 3.790 153 337.94 3.774 118 334.69 3.738 1000 333.81 3.728 981 330.50 3.691 694 329.06 3.675 967 327.19 3.654 469 324.38 3.622 380 322.44 3.601 311 315.75 3.526 36 315.13 3.519 35 314.56 3.513 35 313.50 3.501 32 312.69 3.492 30
in CDCl3
liquid film
4880 A,200 M,liquid
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