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MS-IW-7566 N,N'-bis(2-hydroxyethyl)oxamide C6H12N2O4 (Mass of molecular ion: 176)
Source Temperature: 170 °C Sample Temperature: 190 °C Direct, 75 eV
14.0 1.9 15.0 6.3 16.0 1.0 17.0 3.8 18.0 17.0 19.0 3.7 26.0 6.0 27.0 16.2 28.0 25.1 29.0 17.0 30.0 82.3 31.0 10.3 38.0 1.9 39.0 2.3 40.0 5.3 41.0 11.6 42.0 22.0 43.0 20.3 44.0 25.2 45.0 46.9 46.0 7.7 51.0 1.8 52.0 3.3 53.0 4.7 56.0 5.4 57.0 2.0 58.0 5.7 59.0 5.7 60.0 11.2 61.0 6.7 62.0 2.5 69.0 2.5 70.0 76.9 71.0 5.2 72.0 2.0 87.0 2.0 88.0 100.0 89.0 5.8 98.0 2.1 99.0 1.2 101.0 1.3 103.0 1.2 110.0 1.3 114.0 1.2 115.0 12.2 116.0 1.2 117.0 15.1 118.0 1.4 119.0 11.9 127.0 6.6 128.0 6.4 131.0 1.6 133.0 41.0 134.0 2.6 140.0 4.0 145.0 17.0 146.0 5.4 148.0 1.3 158.0 2.1 176.0 9.0 177.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H12 N2 O4 0.039 g : 0.5 ml DMSO-d6 N,N'-bis(2-hydroxyethyl)oxamide Assign. Shift(ppm)
A 8.57 B 4.75 C 3.459 D 3.223
Hz ppm Int.
3432.13 8.588 150 3426.27 8.574 267 3420.53 8.559 148 1903.93 4.764 419 1898.32 4.750 1000 1892.70 4.736 433 1391.97 3.483 293 1385.86 3.468 879 1380.00 3.454 934 1374.15 3.439 366 1296.75 3.245 362 1290.77 3.230 974 1284.67 3.215 884 1278.44 3.199 282
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