3-氨基-4-甲基苯甲酸甲酯

Mass

MS-IW-9521          
methyl 3-amino-p-toluate
C9H11NO2            (Mass of molecular ion:    165)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.4
      27.0       2.5
      28.0       5.8
      29.0       1.1
      30.0       1.8
      38.0       1.8
      39.0       6.1
      40.0       1.0
      41.0       1.8
      42.0       1.5
      50.0       2.9
      51.0       7.2
      52.0       6.3
      52.5       2.5
      53.0      10.3
      54.0       2.1
      62.0       1.1
      63.0       3.4
      64.0       1.1
      65.0       3.1
      66.0       2.1
      67.0       6.2
      75.0       1.2
      76.0       1.7
      77.0      20.5
      78.0       7.4
      79.0      19.4
      80.0       2.3
      82.5       2.1
      89.0       1.5
      91.0       3.1
      92.0       1.5
      93.0       1.1
     104.0       7.9
     105.0       7.5
     106.0      78.6
     107.0      16.3
     108.0       1.2
     119.0       1.4
     120.0       1.8
     133.0       1.2
     134.0     100.0
     135.0       9.8
     136.0       2.7
     150.0       3.1
     164.0       5.4
     165.0      96.3
     166.0      10.2

Assign. Shift(ppm) A 7.368 B 7.342 C 7.091 D 3.868 E 3.73 F 2.189

     Hz     ppm     Int.

   2949.83   7.382     69
   2948.12   7.377     84
   2942.14   7.362     72
   2940.43   7.358    105
   2935.18   7.345    166
   2933.59   7.341    127
   2837.65   7.101    100
   2829.83   7.081     86
   1546.26   3.870   1000
   1489.14   3.727     69
    875.12   2.190    587