-
MassMS-IW-9726 10-chloro-3-decyne C10H17Cl (Mass of molecular ion: 172)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 11.6 28.0 1.4 29.0 8.3 36.0 2.4 38.0 1.3 39.0 17.2 40.0 5.4 41.0 50.4 42.0 5.8 43.0 8.7 49.0 1.5 50.0 1.3 51.0 4.6 52.0 3.1 53.0 17.7 54.0 5.7 55.0 21.0 56.0 1.8 63.0 3.9 65.0 8.3 66.0 5.4 67.0 100.0 68.0 53.1 69.0 23.6 70.0 1.4 75.0 1.3 77.0 7.4 78.0 1.7 79.0 18.5 80.0 3.5 81.0 39.0 82.0 19.9 83.0 2.4 91.0 6.3 92.0 1.0 93.0 7.4 94.0 2.1 95.0 34.3 96.0 5.7 102.0 1.1 105.0 2.3 107.0 11.0 108.0 1.7 109.0 27.3 110.0 6.1 116.0 1.0 121.0 2.1 123.0 8.3 124.0 1.0 129.0 8.2 130.0 6.7 131.0 3.3 132.0 2.2 136.0 1.4 143.0 9.5 144.0 1.3 145.0 3.2 157.0 1.1 171.0 1.5
400 MHz in CDCl3
-
1H NMR 399.65 MHz C10 H17 Cl 0.05 ml : 0.5 ml CDCl3 10-chloro-3-decyne 
Assign. Shift(ppm)
A 3.534 B 2.16 C 2.15 D 1.779 E 1.49 F 1.43 G 1.111
Hz ppm Int.1419.43 3.552 419 1412.72 3.535 786 1406.01 3.519 441 864.75 2.164 423 862.79 2.159 267 860.60 2.154 232 857.91 2.147 481 857.18 2.145 419 851.68 2.132 228 712.52 1.783 214 573.97 1.437 290 572.75 1.434 284 570.19 1.427 361 567.38 1.420 327 451.66 1.131 461 444.09 1.112 1000 436.65 1.093 436
in CDCl3
liquid film
更多供应商