图谱信息 供应商 相关产品
网站主页CAS数据库列表 18295-64-2更多图谱10-氯-3-癸炔(18295-64-2)核磁图(1HNMR)

10-氯-3-癸炔

产品名称 10-氯-3-癸炔

CAS号18295-64-2

分子式C10H17Cl

分子量172.7

展开


  • Mass

    MS-IW-9726          
    10-chloro-3-decyne
    C10H17Cl            (Mass of molecular ion:    172)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0      11.6
          28.0       1.4
          29.0       8.3
          36.0       2.4
          38.0       1.3
          39.0      17.2
          40.0       5.4
          41.0      50.4
          42.0       5.8
          43.0       8.7
          49.0       1.5
          50.0       1.3
          51.0       4.6
          52.0       3.1
          53.0      17.7
          54.0       5.7
          55.0      21.0
          56.0       1.8
          63.0       3.9
          65.0       8.3
          66.0       5.4
          67.0     100.0
          68.0      53.1
          69.0      23.6
          70.0       1.4
          75.0       1.3
          77.0       7.4
          78.0       1.7
          79.0      18.5
          80.0       3.5
          81.0      39.0
          82.0      19.9
          83.0       2.4
          91.0       6.3
          92.0       1.0
          93.0       7.4
          94.0       2.1
          95.0      34.3
          96.0       5.7
         102.0       1.1
         105.0       2.3
         107.0      11.0
         108.0       1.7
         109.0      27.3
         110.0       6.1
         116.0       1.0
         121.0       2.1
         123.0       8.3
         124.0       1.0
         129.0       8.2
         130.0       6.7
         131.0       3.3
         132.0       2.2
         136.0       1.4
         143.0       9.5
         144.0       1.3
         145.0       3.2
         157.0       1.1
         171.0       1.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H17 Cl 0.05 ml : 0.5 ml CDCl3
    10-chloro-3-decyne
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.534 B 2.16 C 2.15 D 1.779 E 1.49 F 1.43 G 1.111

         Hz     ppm     Int.
    

       1419.43   3.552    419
       1412.72   3.535    786
       1406.01   3.519    441
        864.75   2.164    423
        862.79   2.159    267
        860.60   2.154    232
        857.91   2.147    481
        857.18   2.145    419
        851.68   2.132    228
        712.52   1.783    214
        573.97   1.437    290
        572.75   1.434    284
        570.19   1.427    361
        567.38   1.420    327
        451.66   1.131    461
        444.09   1.112   1000
        436.65   1.093    436
    

in CDCl3



liquid film