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MS-IW-6980 trichloroisobutylsilane C4H9Cl3Si (Mass of molecular ion: 190)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 7.5 28.0 1.0 29.0 4.3 38.0 1.0 39.0 11.1 40.0 1.7 41.0 21.4 42.0 4.1 43.0 55.0 44.0 1.9 49.0 1.0 53.0 1.2 55.0 3.7 56.0 4.4 57.0 3.9 63.0 8.8 65.0 3.4 98.0 2.4 99.0 2.5 100.0 1.8 101.0 1.8 112.0 2.3 113.0 4.5 114.0 1.8 115.0 3.0 117.0 1.1 125.0 1.3 133.0 55.8 134.0 2.9 135.0 55.8 136.0 2.9 137.0 19.7 138.0 2.1 139.0 31.9 140.0 3.7 141.0 20.6 142.0 2.0 143.0 3.9 153.0 1.4 154.0 2.8 155.0 2.4 156.0 2.0 157.0 1.1 174.0 1.1 175.0 100.0 176.0 9.6 177.0 99.7 178.0 8.7 179.0 34.3 180.0 2.8 181.0 4.4 189.0 1.9 191.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H9 Cl3 Si 0.05 ml : 0.5 ml CDCl3 trichloroisobutylsilane Assign. Shift(ppm)
A 2.108 B 1.418 C 1.073
Hz ppm Int.
856.20 2.143 43 849.49 2.126 84 842.77 2.109 106 836.06 2.092 90 829.35 2.076 50 570.19 1.427 487 563.23 1.410 465 560.91 1.404 21 432.50 1.083 1000 429.81 1.076 60 425.54 1.065 954 421.39 1.055 46
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