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网站主页CAS数据库列表 1805-32-9更多图谱3,4-二氯苄醇(1805-32-9)红外图谱(IR1)

3,4-二氯苄醇

产品名称 3,4-二氯苄醇

CAS号1805-32-9

分子式C7H6Cl2O

分子量177.03

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  • Mass

    MS-NW-7525          
    3,4-dichlorobenzyl alcohol
    C7H6Cl2O            (Mass of molecular ion:    176)
    

       Source Temperature: 210 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       2.2
          29.0       8.0
          31.0       8.0
          36.0       2.0
          37.0       4.0
          38.0       5.8
          39.0       4.6
          43.0       2.9
          44.0       1.6
          49.0       2.8
          50.0      13.2
          51.0      16.4
          52.0      12.7
          52.5       1.5
          53.0       1.4
          55.0       2.2
          56.0       3.5
          57.0       1.1
          60.0       1.6
          61.0       5.1
          61.5       1.2
          62.0       5.5
          63.0       6.4
          70.0       3.9
          70.5       1.3
          71.0       1.5
          72.0       1.9
          73.0       8.2
          74.0      14.5
          75.0      27.8
          76.0       4.3
          77.0     100.0
          78.0       9.6
          84.0       4.9
          85.0       5.7
          86.0       3.4
          87.0       3.7
          87.5       3.0
          88.0       1.4
          88.5       2.0
          89.0       4.7
          97.0       2.2
          99.0       1.8
         105.0       2.0
         108.0       1.0
         109.0       8.3
         110.0       3.4
         111.0      63.3
         112.0      12.2
         113.0      58.0
         114.0       6.7
         115.0      12.9
         116.0       1.1
         123.0      10.3
         124.0       2.8
         125.0       3.8
         126.0       1.0
         133.0       1.6
         135.0       1.1
         139.0      12.1
         140.0       5.3
         141.0      96.7
         142.0       9.1
         143.0      31.1
         144.0       2.8
         145.0       6.7
         146.0       3.0
         147.0      23.7
         148.0       3.4
         149.0      13.9
         150.0       1.3
         151.0       2.3
         159.0      13.4
         160.0       1.7
         161.0       8.7
         163.0       1.7
         173.0       4.0
         175.0      15.2
         176.0      66.0
         177.0      13.9
         178.0      43.6
         179.0       5.0
         180.0       7.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H6 Cl2 O 0.039 g : 0.5 ml CDCl3
    3,4-dichlorobenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.42 B 7.39 C 7.147 D 4.608 E 2.35 J(A,C)=1.9HZ J(B,C)=8.3HZ J(C,D)=0.6HZ

         Hz     ppm     Int.
    

        666.63   7.444    522
        665.88   7.436    444
        665.50   7.431    445
        664.69   7.422    358
        663.88   7.413    448
        663.50   7.409    474
        658.63   7.355    763
        654.69   7.311     51
        652.69   7.288     33
        651.94   7.280     33
        651.81   7.278     33
        651.38   7.274     33
        650.31   7.262     31
        649.50   7.253     30
        649.13   7.248     30
        644.50   7.197    239
        643.88   7.190    405
        643.25   7.183    252
        642.56   7.175    233
        641.94   7.168    345
        641.25   7.161    198
        638.94   7.135     39
        638.38   7.128     36
        636.25   7.105    125
        635.63   7.098    208
        635.00   7.091    135
        634.31   7.083    125
        633.69   7.076    185
        633.06   7.069    108
        412.75   4.609   1000
        405.06   4.523     41
        402.81   4.498     32
        210.63   2.352    153
    

in CDCl3



KBr disc



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