-
MassMS-NW-6268 bicyclo(3.3.1)nonan-9-one C9H14O (Mass of molecular ion: 138)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.2 18.0 2.0 26.0 1.8 27.0 20.8 28.0 1.1 29.0 8.4 38.0 1.7 39.0 25.1 40.0 5.1 41.0 39.6 42.0 3.1 43.0 2.1 50.0 1.6 51.0 3.7 52.0 2.1 53.0 10.0 54.0 42.1 55.0 15.7 56.0 3.9 57.0 1.5 63.0 1.1 65.0 3.6 66.0 9.6 67.0 100.0 68.0 24.6 69.0 9.4 70.0 2.7 77.0 3.2 78.0 4.4 79.0 12.4 80.0 3.9 81.0 26.2 82.0 58.4 83.0 5.9 84.0 3.5 91.0 15.1 92.0 16.4 93.0 2.5 94.0 4.2 95.0 10.8 96.0 3.6 97.0 2.2 105.0 3.2 107.0 1.2 109.0 3.4 110.0 19.3 111.0 1.8 119.0 1.1 120.0 12.7 121.0 1.6 138.0 53.8 139.0 6.2
90 MHz in CDCl3
-
1H NMR 89.56 MHz C9 H14 O 0.041 g : 0.5 ml CDCl3 bicyclo(3.3.1)nonan-9-one 
Assign. Shift(ppm)
A 2.42 B 2.13 to 1.97 C 1.72 to 1.42 CHEMICALLY EXCHANGING SYSTEM.
Hz ppm Int.216.88 2.422 135 213.94 2.389 103 209.25 2.337 30 207.69 2.320 32 202.13 2.257 31 196.31 2.192 34 195.75 2.186 30 195.25 2.181 30 194.75 2.175 30 191.19 2.135 134 185.94 2.077 1000 184.63 2.062 803 177.25 1.980 161 174.13 1.945 86 171.94 1.920 59 170.06 1.899 43 169.63 1.895 41 151.06 1.687 30 150.88 1.685 30 148.13 1.654 35 143.81 1.606 60 141.44 1.580 33 138.75 1.550 82 136.63 1.526 53 134.69 1.504 117
in CDCl3
KBr disc
nujol mull
更多供应商