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MS-IW-5092 trimethyl(phenylthiomethyl)silane C10H16SSi (Mass of molecular ion: 196)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 1.0 31.0 1.1 39.0 1.2 43.0 5.4 44.0 3.7 45.0 10.2 51.0 3.6 57.0 1.3 58.0 1.2 59.0 4.8 65.0 2.6 72.0 5.2 73.0 100.0 74.0 10.6 75.0 5.7 77.0 6.2 78.0 1.0 79.0 1.0 90.5 1.1 91.0 15.3 92.0 1.2 105.0 6.8 107.0 1.0 109.0 1.5 121.0 1.1 135.0 11.8 136.0 1.7 137.0 2.8 151.0 4.1 153.0 1.0 165.0 18.3 166.0 3.0 167.0 2.3 181.0 39.9 182.0 6.3 183.0 3.6 196.0 34.9 197.0 6.0 198.0 3.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H16 S Si 0.05 ml : 0.5 ml CDCl3 trimethyl(phenylthiomethyl)silane Assign. Shift(ppm)
A 7.265 B 7.234 C 7.072 D 2.155 E 0.155
Hz ppm Int.
2910.64 7.283 53 2908.94 7.279 72 2906.98 7.274 33 2904.17 7.267 55 2901.98 7.262 191 2900.63 7.258 170 2897.58 7.251 167 2895.14 7.245 38 2890.38 7.233 146 2888.55 7.228 66 2883.91 7.217 33 2882.08 7.212 64 2834.47 7.093 31 2833.01 7.089 53 2831.30 7.085 30 2825.93 7.072 70 2824.83 7.069 38 2824.10 7.067 30 2819.09 7.054 37 864.26 2.163 42 861.33 2.156 413 65.06 0.163 244 61.89 0.155 1000 58.35 0.147 165
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