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网站主页CAS数据库列表 17784-47-3更多图谱盐酸丫啶(17784-47-3)红外图谱(IR1)

盐酸丫啶

产品名称 盐酸丫啶

CAS号17784-47-3

分子式C13H10ClN

分子量215.68

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  • Mass

    MS-NW-0252          
    acridine hydrochloride
    C13H9N HCl          (Mass of molecular ion:    179)
    

       Source Temperature: 160 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          17.0       1.7
          18.0       8.4
          36.0       4.2
          38.0       1.3
          39.0       1.2
          50.0       1.9
          51.0       1.8
          62.0       1.1
          63.0       3.0
          74.0       1.7
          75.0       3.9
          75.5       1.8
          76.0       4.5
          77.0       1.0
          87.0       1.0
          88.5       1.0
          89.0       8.6
          89.5       8.2
          90.0       1.1
         101.0       1.1
         125.0       1.3
         126.0       2.0
         127.0       1.7
         150.0       3.1
         151.0       7.0
         152.0       6.9
         153.0       4.2
         176.0       1.0
         177.0       5.8
         178.0      15.8
         179.0     100.0
         180.0      14.0
         181.0       1.2
    

90 MHz in D2O

400 MHz in D2O (at 60.9C)


  • 1H NMR 89.56 MHz
    C13 H9 N 0.043 g : 0.5 ml D2O
    acridine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.607 B 7.74 C 7.56 D 7.47 E 7.39 400MHZ : HSP-42-318 THE SOLVENT SIGNAL REMOVED.

         Hz     ppm     Int.
    

        770.63   8.605    660
        703.00   7.850    214
        701.31   7.831    249
        696.38   7.776    367
        694.88   7.759    501
        692.31   7.731    420
        688.00   7.683    477
        686.19   7.662    600
        683.31   7.630    336
        675.94   7.548   1000
        668.81   7.468    535
        667.81   7.457    754
        663.63   7.410    813
        662.50   7.398    854
        661.25   7.384    513
        660.25   7.373    380
        658.88   7.357    183
        655.31   7.317    533
        654.38   7.307    499
    


  • 1H NMR 399.65 MHz
    C13 H9 N 0.036 g : 0.5 ml D2O at 60C
    acridine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.850 B 7.897 C 7.794 D 7.632 E 7.546 THE SOLVENT PEAK REMOVED.

         Hz     ppm     Int.
    

       3536.99   8.851    813
       3168.58   7.929     43
       3167.60   7.926     50
       3164.92   7.920    417
       3163.57   7.916    492
       3158.20   7.903    499
       3156.25   7.898    724
       3154.79   7.894    614
       3149.41   7.881    532
       3148.07   7.878    609
       3128.17   7.828     33
       3127.69   7.827     35
       3127.32   7.826     37
       3119.87   7.807    731
       3119.14   7.805    720
       3115.72   7.797     89
       3114.75   7.794     95
       3111.33   7.786    859
       3110.72   7.784    827
       3064.94   7.670     30
       3064.58   7.669     30
       3063.48   7.666     32
       3062.87   7.664     33
       3062.38   7.663     35
       3061.77   7.662     39
       3061.40   7.661     41
       3060.67   7.659     48
       3054.57   7.644    863
       3053.83   7.642   1000
       3050.05   7.632     80
       3049.32   7.630     78
       3045.90   7.622    738
       3045.04   7.620    840
       3041.14   7.610     37
       3040.77   7.609     33
       3040.28   7.608     30
       3031.86   7.587     30
       3031.49   7.586     32
       3031.25   7.585     32
       3030.76   7.584     33
       3029.91   7.582     35
       3029.54   7.581     37
       3028.56   7.579     46
       3026.73   7.574     61
       3023.32   7.565    558
       3022.46   7.563    609
       3019.17   7.555     89
       3016.60   7.549    551
       3015.14   7.545    694
       3014.04   7.542    579
       3010.74   7.534     58
       3009.89   7.532     61
       3008.06   7.527    421
       3007.20   7.525    456
    

KBr disc



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