2,4-二氯苄醇

Mass

MS-NW-6530          
2,4-dichlorobenzyl alcohol
C7H6Cl2O            (Mass of molecular ion:    176)

   Source Temperature: 240 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.7
      27.0       2.0
      28.0       4.2
      29.0       7.3
      31.0       6.9
      36.0       3.5
      37.0       4.1
      38.0       6.1
      39.0       3.9
      43.0       2.6
      44.0       1.7
      49.0       2.7
      50.0      13.2
      51.0      16.3
      52.0      12.8
      52.5       1.2
      53.0       1.2
      55.0       1.6
      56.0       2.9
      57.0       1.0
      60.0       1.4
      61.0       4.6
      61.5       1.0
      62.0       5.3
      63.0       5.9
      70.0       3.1
      70.5       1.2
      71.0       1.1
      72.0       1.4
      73.0       6.9
      74.0      13.2
      75.0      28.7
      76.0       5.3
      77.0      87.8
      78.0       8.8
      84.0       3.4
      85.0       5.3
      86.0       2.7
      87.0       2.9
      87.5       2.2
      88.0       1.0
      88.5       1.3
      89.0       4.6
      97.0       1.7
      99.0       1.7
     105.0       2.3
     109.0       6.0
     110.0       3.3
     111.0      54.8
     112.0       9.8
     113.0      51.5
     114.0       5.5
     115.0      12.1
     123.0       8.3
     124.0       2.6
     125.0       3.4
     133.0       1.2
     139.0      19.1
     140.0      14.7
     141.0     100.0
     142.0      12.4
     143.0      30.1
     144.0       2.7
     145.0       5.0
     146.0       2.8
     147.0      16.3
     148.0       2.6
     149.0       9.3
     150.0       1.0
     151.0       1.5
     159.0      16.8
     160.0       2.0
     161.0      11.0
     162.0       1.2
     163.0       1.9
     173.0       5.3
     174.0       1.7
     175.0      21.1
     176.0      60.6
     177.0      16.4
     178.0      39.8
     179.0       5.0
     180.0       6.4

Assign. Shift(ppm) A 7.38 B 7.36 C 7.25 D 4.709 E 2.31 J(A,C)=8.1HZ. J(B,C)=2.1HZ.

     Hz     ppm     Int.

    668.06   7.460    114
    667.63   7.455    119
    659.38   7.363    590
    657.69   7.344    469
    654.38   7.307     52
    652.44   7.285    357
    650.31   7.262    237
    647.94   7.235     37
    647.50   7.230     32
    647.06   7.225     32
    644.38   7.195    108
    642.31   7.172     95
    421.75   4.710   1000
    416.44   4.650     32
    206.50   2.306    507