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MassMS-IW-1752 2-amino-5-nitrobenzophenone C13H10N2O3 (Mass of molecular ion: 242)
Source Temperature: 140 °C Sample Temperature: 100 °C Direct, 75 eV
28.0 1.9 38.0 1.1 39.0 2.4 41.0 2.1 50.0 2.8 51.0 11.7 52.0 7.3 53.0 1.8 62.0 2.1 63.0 5.6 64.0 4.2 65.0 2.6 70.5 1.0 74.0 1.6 75.0 1.9 76.0 2.4 77.0 56.5 78.0 4.9 79.0 1.2 83.5 3.3 89.0 1.8 90.0 2.7 91.0 13.1 92.0 1.5 98.0 2.8 105.0 57.2 106.0 5.5 107.0 1.6 115.0 2.8 119.0 18.1 120.0 1.5 121.0 1.0 128.0 1.2 139.0 4.9 140.0 3.0 141.0 4.3 151.0 3.8 152.0 2.0 153.0 1.3 156.0 1.3 164.0 1.3 165.0 29.9 166.0 7.8 167.0 15.1 168.0 4.7 169.0 1.0 177.0 1.1 178.0 1.8 179.0 3.1 183.0 3.0 184.0 1.2 194.0 3.4 195.0 34.7 196.0 10.5 197.0 1.2 212.0 1.7 213.0 2.0 224.0 2.0 225.0 6.1 226.0 2.3 241.0 89.0 242.0 100.0 243.0 14.5 244.0 1.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H10 N2 O3 0.039 g : 0.5 ml DMSO-d6 2-amino-5-nitrobenzophenone 
Assign. Shift(ppm)
A 8.24 B 8.228 C 8.136 D 7.68 E 7.591 F 6.997
Hz ppm Int.3292.36 8.239 417 3289.67 8.232 839 3286.99 8.225 814 3275.51 8.196 30 3257.69 8.152 351 3255.00 8.145 303 3248.41 8.129 365 3245.73 8.122 333 3078.61 7.704 67 3077.27 7.700 149 3075.81 7.697 122 3074.58 7.694 87 3072.63 7.689 390 3071.29 7.685 561 3069.95 7.682 780 3067.99 7.677 207 3066.53 7.674 251 3063.72 7.667 1000 3062.74 7.664 916 3056.15 7.648 31 3041.38 7.611 647 3038.21 7.603 132 3035.03 7.595 508 3034.30 7.593 519 3031.62 7.586 182 3028.08 7.577 123 3026.61 7.574 288 3025.63 7.571 179 3024.17 7.568 53 2801.27 7.010 723 2791.87 6.986 699
DMSO-d6
KBr disc
nujol mull
4880 A,200 M,powder
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