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MS-IW-0802 bis(pentafluorophenyl)methanol C13H2F10O (Mass of molecular ion: 364)
Source Temperature: 180 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 10.3 93.0 2.6 98.0 1.5 99.0 5.4 117.0 6.3 119.0 4.4 123.5 1.1 129.0 1.2 139.0 1.5 148.0 2.2 149.0 5.1 167.0 7.9 168.0 7.5 169.0 6.6 171.5 1.1 177.0 11.6 178.0 1.4 195.0 34.6 196.0 13.8 197.0 100.0 198.0 7.7 215.0 1.3 247.0 1.7 278.0 6.3 296.0 1.2 297.0 2.2 309.0 1.6 327.0 1.9 344.0 7.1 345.0 1.3 347.0 6.5 348.0 1.1 363.0 1.7 364.0 58.7 365.0 8.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H2 F10 O 0.039 g : 0.5 ml CDCl3 bis(pentafluorophenyl)methanol Assign. Shift(ppm)
A 6.50 B 3.371
Hz ppm Int.
2604.13 6.517 973 2593.87 6.491 1000 1356.81 3.395 86 1354.74 3.390 302 1352.66 3.385 449 1350.59 3.380 316 1348.51 3.375 103 1346.56 3.370 92 1344.48 3.365 293 1342.41 3.359 434 1340.33 3.354 309 1338.26 3.349 99
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