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MS-NW-1355 (3-(2-aminoethylamino)propyl)trimethoxysilane C8H22N2O3Si (Mass of molecular ion: 222)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 6.4 18.0 3.8 27.0 1.2 28.0 6.4 29.0 13.4 30.0 11.2 31.0 28.8 32.0 20.3 39.0 1.0 41.0 2.9 42.0 3.0 43.0 5.7 44.0 19.1 45.0 1.1 55.0 1.1 56.0 2.8 57.0 1.4 59.0 6.7 60.0 1.4 61.0 5.3 70.0 1.6 71.0 1.0 73.0 8.1 74.0 1.7 75.0 1.0 76.0 1.0 77.0 1.6 85.0 1.2 90.0 2.1 91.0 14.9 92.0 1.3 99.0 1.0 100.0 1.9 101.0 1.1 103.0 1.2 104.0 1.3 106.0 1.4 107.0 1.3 116.0 1.2 117.0 1.2 118.0 2.8 120.0 1.2 121.0 15.7 122.0 1.6 128.0 1.2 130.0 30.7 131.0 4.6 132.0 2.1 136.0 1.4 146.0 1.6 147.0 1.1 148.0 3.0 149.0 1.3 157.0 1.6 158.0 1.8 159.0 2.3 160.0 100.0 161.0 12.8 162.0 4.9 192.0 27.5 193.0 3.9 194.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H22 N2 O3 Si 0.04 ml : 0.5 ml CDCl3 (3-(2-aminoethylamino)propyl)trimethoxysilane Assign. Shift(ppm)
A 3.570 B 2.90 to 2.52 C 1.60 D 1.25 E 0.67
Hz ppm Int.
319.69 3.570 1000 318.56 3.557 62 250.63 2.799 26 249.81 2.790 21 246.69 2.755 35 245.81 2.745 51 242.81 2.712 43 242.06 2.703 49 238.94 2.668 22 238.19 2.660 26 235.06 2.625 30 233.88 2.612 21 227.81 2.544 24 111.69 1.248 62
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