-
MassMS-IW-8166 3,5-diisopropylpyrazole C9H16N2 (Mass of molecular ion: 152)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.3 28.0 1.5 39.0 2.9 41.0 6.4 42.0 2.2 43.0 5.7 53.0 1.6 54.0 1.6 60.0 1.6 60.5 2.1 61.0 2.5 65.0 1.1 66.0 1.5 67.0 2.7 68.0 3.8 69.0 2.5 77.0 1.5 81.0 3.0 82.0 1.1 91.0 1.0 93.0 1.1 95.0 49.8 96.0 3.4 107.0 1.0 109.0 10.7 110.0 1.6 121.0 5.8 122.0 3.3 123.0 1.3 124.0 15.7 125.0 1.4 135.0 3.6 137.0 100.0 138.0 9.8 150.0 1.0 151.0 14.8 152.0 40.9 153.0 7.5
400 MHz in CDCl3
-
1H NMR 399.65 MHz C9 H16 N2 0.041 g : 0.5 ml CDCl3 3,5-diisopropylpyrazole 
Assign. Shift(ppm)
A 5.853 B 2.940 C 1.57 D 1.247
Hz ppm Int.2339.23 5.854 163 1189.45 2.977 28 1182.37 2.959 68 1175.54 2.942 92 1168.58 2.925 72 1161.62 2.907 31 625.85 1.566 223 501.95 1.256 1000 498.66 1.248 95 495.00 1.239 973
in CDCl3
KBr disc
nujol mull
更多供应商
