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MS-IW-4087 (S)-(-)-alpha-methyldibenzylamine C15H17N (Mass of molecular ion: 211)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.0 42.0 1.3 51.0 1.8 65.0 6.1 77.0 6.3 78.0 1.8 79.0 5.5 89.0 1.1 91.0 100.0 92.0 9.8 103.0 3.1 104.0 3.7 105.0 16.3 106.0 8.2 120.0 2.4 134.0 5.3 196.0 74.3 197.0 11.7 210.0 1.0 211.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H17 N 0.05 ml : 0.5 ml CDCl3 (S)-(-)-alpha-methyldibenzylamine Assign. Shift(ppm)
A 7.32 to 7.20 B 3.776 C *1 3.626 D *1 3.568 E 1.58 F 1.330
Hz ppm Int.
2935.06 7.345 87 2932.98 7.339 139 2930.66 7.334 84 2926.64 7.324 712 2925.66 7.321 711 2919.31 7.305 368 2918.58 7.303 446 2916.63 7.298 147 2913.94 7.292 91 2912.72 7.289 164 2911.38 7.285 148 2910.64 7.283 165 2909.42 7.280 56 2907.47 7.276 133 2905.52 7.271 360 2904.66 7.269 310 2901.00 7.259 433 2898.93 7.254 933 2894.17 7.242 105 2892.46 7.238 142 2890.26 7.232 142 2888.18 7.227 194 2885.99 7.222 98 2884.28 7.218 104 2882.20 7.212 208 2881.59 7.211 218 2880.13 7.207 182 2879.03 7.204 136 2876.46 7.198 141 2875.12 7.195 152 2873.29 7.190 156 2870.12 7.182 85 2867.31 7.175 68 2864.87 7.169 40 1516.60 3.795 73 1510.01 3.779 228 1503.42 3.762 230 1496.83 3.746 78 1456.30 3.644 157 1443.24 3.612 366 1427.49 3.572 414 1414.31 3.539 171 631.10 1.580 64 534.91 1.339 1000 528.32 1.322 992
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