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网站主页CAS数据库列表 17420-30-3更多图谱2-氰基-4-硝基苯胺(17420-30-3)Raman光谱

2-氰基-4-硝基苯胺

产品名称 2-氰基-4-硝基苯胺

CAS号17420-30-3

分子式C7H5N3O2

分子量163.13

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  • Mass

    MS-IW-0859          
    5-nitroanthranilonitrile
    C7H5N3O2            (Mass of molecular ion:    163)
    

       Source Temperature: 170 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          28.0       4.1
          30.0       2.0
          37.0       1.1
          38.0       2.4
          39.0       6.5
          40.0       1.1
          41.0       2.2
          50.0       1.3
          51.0       2.6
          52.0       4.2
          53.0       1.2
          61.0       1.3
          62.0       3.6
          63.0      20.9
          64.0       5.6
          65.0       2.1
          66.0       1.9
          76.0       1.0
          77.0       1.4
          78.0       3.6
          88.0       1.9
          89.0       3.2
          90.0      60.1
          91.0       5.0
         105.0       6.9
         106.0       1.1
         116.0       2.5
         117.0      38.1
         118.0       3.4
         133.0      17.7
         134.0       1.5
         147.0       2.8
         163.0     100.0
         164.0       9.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H5 N3 O2 0.036 g : 0.5 ml DMSO-d6
    5-nitroanthranilonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.385 B 8.130 C 7.50 D 6.872

         Hz     ppm     Int.
    

       3352.42   8.389    962
       3349.73   8.382   1000
       3343.38   8.366     23
       3341.55   8.362     23
       3255.62   8.147    507
       3252.93   8.140    474
       3246.22   8.123    531
       3243.53   8.116    509
       2999.39   7.506    415
       2751.34   6.885    905
       2746.58   6.873     41
       2741.94   6.861    893
       2737.30   6.850     29
    

in DMSO-d6



KBr disc



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