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网站主页CAS数据库列表 17301-94-9更多图谱4-甲基壬烷(17301-94-9)核磁图(1HNMR)

4-甲基壬烷

产品名称 4-甲基壬烷

CAS号17301-94-9

分子式C10H22

分子量142.28

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  • Mass

    MS-IW-2662          
    4-methylnonane
    C10H22              (Mass of molecular ion:    142)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0       9.3
          28.0       1.0
          29.0      15.9
          39.0       6.8
          40.0       1.2
          41.0      29.2
          42.0      12.8
          43.0      87.2
          44.0       3.5
          53.0       1.9
          54.0       1.0
          55.0      20.3
          56.0      10.8
          57.0     100.0
          58.0       5.8
          69.0       5.1
          70.0      55.5
          71.0      60.0
          72.0       3.3
          83.0       1.4
          84.0       2.3
          85.0       7.6
          98.0      23.9
          99.0      14.5
         100.0       1.0
         112.0       3.2
         113.0       2.5
         127.0       1.4
         142.0       4.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H22 0.05 ml : 0.5 ml CDCl3
    4-methylnonane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.39 B 1.35 C 1.32 D 1.32 to 1.24 E 1.24 F 1.22 G 1.10 J 1.07 K 0.885 L 0.877 M 0.842 90MHZ : HSP-04-006

         Hz     ppm     Int.
    

        570.31   1.428     30
        568.73   1.424     31
        563.96   1.412     48
        561.40   1.405     57
        557.98   1.397     75
        556.88   1.394     69
        556.40   1.393     69
        554.08   1.387     84
        552.73   1.384     76
        551.39   1.380     92
        550.05   1.377     76
        548.58   1.373     80
        546.51   1.368     80
        545.78   1.366     78
        543.82   1.361     87
        541.14   1.355     95
        538.33   1.348    110
        536.38   1.343    105
        533.94   1.337    104
        531.86   1.331    151
        531.25   1.330    154
        529.54   1.326    139
        524.54   1.313    208
        523.93   1.311    214
        521.85   1.306    244
        518.43   1.298    313
        516.48   1.293    291
        515.26   1.290    345
        512.21   1.282    279
        509.52   1.275    343
        506.84   1.269    504
        502.93   1.259    370
        500.37   1.253    318
        498.66   1.248    272
        496.58   1.243    296
        491.33   1.230    237
        487.67   1.221    131
        487.06   1.219    133
        484.01   1.212     81
        481.81   1.206     72
        479.49   1.200     37
        476.81   1.194     35
        448.73   1.123     44
        447.75   1.121     47
        445.19   1.114     64
        443.73   1.111     48
        440.55   1.103     84
        438.11   1.097    139
        435.18   1.089    115
        432.74   1.083    110
        430.54   1.078    109
        427.37   1.070    116
        425.17   1.064     85
        423.10   1.059     59
        422.36   1.057     58
        419.80   1.051     49
        418.09   1.047     38
        416.75   1.043     34
        415.28   1.040     35
        360.60   0.903    493
        357.67   0.895    444
        353.88   0.886    829
        350.59   0.878    773
        348.27   0.872    235
        346.56   0.868    490
        343.38   0.860    415
        339.72   0.851   1000
        333.13   0.834    970
    


  • 1H NMR 89.56 MHz
    C10 H22 0.04 ml : 0.5 ml CDCl3
    4-methylnonane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.39 B *1 1.35 C *1 1.32 D *1 1.32 to 1.24 E *2 1.24 F *3 1.22 G *2 1.10 J *3 1.07 K 0.885 L 0.877 M 0.840 THE SHIFT VALUES WERE OBTAINED AT 400MHZ.

         Hz     ppm     Int.
    

        133.63   1.493     34
        133.25   1.488     34
        131.69   1.471     35
        130.88   1.462     38
        129.94   1.451     42
        119.50   1.335    244
        112.38   1.255    847
         99.69   1.114     94
         97.81   1.093     99
         95.00   1.061     83
         92.38   1.032     63
         91.88   1.026     63
         91.38   1.021     63
         91.00   1.017     62
         90.50   1.011     64
         89.50   1.000     70
         84.56   0.945    326
         78.50   0.877   1000
         72.44   0.809    563
    

in CDCl3



liquid film