2-氯-6-甲氧基吡啶

Mass

MS-NW-1318          
2-chloro-6-methoxypyridine
C6H6ClNO            (Mass of molecular ion:    143)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       7.5
      18.0       1.4
      26.0       4.4
      27.0       3.5
      28.0       5.2
      29.0       2.8
      32.0       1.3
      36.0       1.1
      37.0       8.8
      38.0      20.6
      39.0      38.9
      40.0       2.1
      42.0       1.1
      47.0       1.2
      49.0       3.6
      50.0      10.5
      51.0      11.7
      52.0       5.4
      53.0       4.9
      54.0       1.0
      60.0       1.6
      61.0       1.7
      62.0       2.2
      63.0       2.8
      64.0      11.8
      65.0      12.8
      66.0       3.2
      67.0       1.0
      73.0       3.3
      74.0       1.9
      75.0       3.9
      76.0      14.8
      77.0       6.9
      78.0      79.4
      79.0       7.7
      80.0       3.7
      85.0       3.2
      86.0       4.4
      87.0       1.5
      88.0       1.4
      93.0      17.5
      94.0       2.9
     100.0       5.1
     102.0       2.1
     106.0       3.2
     107.0       1.0
     108.0      11.2
     109.0       3.7
     110.0       1.6
     112.0       9.9
     113.0      78.0
     114.0      36.6
     115.0      27.3
     116.0      11.1
     138.0       5.2
     139.0       5.9
     140.0       1.4
     142.0     100.0
     143.0      83.7
     144.0      36.5
     145.0      26.3
     146.0       1.9

Assign. Shift(ppm) A 7.50 B 6.89 C 6.65 D 3.93

     Hz     ppm     Int.

    679.31   7.585     69
    671.81   7.502     98
    671.19   7.495     91
    663.69   7.411    106
    620.06   6.924    105
    619.38   6.916    112
    612.63   6.841     86
    611.88   6.833     81
    598.75   6.686    111
    598.06   6.678    101
    590.63   6.595     88
    589.94   6.588     82
    351.81   3.929   1000