Phenothiazine, 10-[3-(dimethylamino)-2-methylpropyl]-2-methoxy-, maleate (1:1) (8CI)
产品名称 Phenothiazine, 10-[3-(dimethylamino)-2-methylpropyl]-2-methoxy-, maleate (1:1) (8CI)
CAS号17086-29-2
分子式C23H28N2O5S
分子量444.54382
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MassMS-IW-3599 10-(3-dimethylamino-2-methylpropyl)-2-methoxyphenothiazine maleate C19H24N2OS C4H4O4 (Mass of molecular ion: 328)
Source Temperature: 180 °C Sample Temperature: 200 °C Direct, 75 eV
18.0 4.0 26.0 4.8 27.0 2.3 28.0 1.5 29.0 1.3 30.0 2.2 39.0 1.1 41.0 1.8 42.0 4.0 43.0 1.8 44.0 3.4 45.0 3.9 53.0 1.2 54.0 4.5 55.0 2.4 57.0 1.5 58.0 100.0 59.0 5.8 63.0 1.0 69.0 1.3 70.0 1.2 71.0 1.4 72.0 5.2 77.0 1.0 84.0 4.3 85.0 1.6 86.0 2.0 98.0 1.7 99.0 2.3 100.0 16.9 101.0 1.3 141.0 1.0 167.0 2.2 184.0 1.1 185.0 7.8 186.0 3.0 198.0 1.9 199.0 1.6 210.0 4.7 211.0 1.1 214.0 1.2 227.0 1.5 228.0 9.3 229.0 10.8 230.0 2.0 242.0 8.6 243.0 5.4 244.0 1.2 268.0 3.5 269.0 3.1 270.0 2.8 282.0 5.6 283.0 7.5 284.0 1.7 328.0 46.0 329.0 10.3 330.0 3.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C19 H24 N2 O S 0.039 g : 0.5 ml DMSO-d6 10-(3-dimethylamino-2-methylpropyl)-2-methoxyphenothiazine maleate 
Assign. Shift(ppm)
A 9. B 7.24 C 7.22 D 7.110 E 7.11 F 6.996 G 6.686 J 6.617 K 6.074 L *1 3.933 M *1 3.79 N 3.761 P *2 3.130 Q *2 3.036 R 2.721 S 2.35 T 1.051 J(L,M)=13.9HZ J(L,S)=6.8HZ J(M,S)=8.0HZ J(P,Q)=12.8HZ J(P,S)=4.5HZ J(Q,S)=8.4HZ
Hz ppm Int.2901.91 7.262 30 2896.05 7.247 38 2894.58 7.243 54 2893.85 7.241 55 2889.27 7.230 79 2887.99 7.227 93 2886.52 7.223 60 2881.58 7.211 94 2880.29 7.208 65 2846.22 7.122 164 2844.03 7.117 73 2837.80 7.101 183 2803.73 7.016 42 2802.63 7.013 43 2796.22 6.997 69 2795.49 6.995 66 2788.89 6.979 35 2787.79 6.976 34 2673.86 6.691 87 2671.30 6.685 105 2649.87 6.631 73 2647.49 6.625 61 2641.44 6.610 66 2638.88 6.603 60 2427.51 6.075 1000 1569.92 3.929 32 1563.14 3.912 32 1527.79 3.823 30 1519.92 3.804 33 1503.43 3.762 739 1248.46 3.124 36 1243.88 3.113 35 1222.64 3.060 31 1214.21 3.039 34 1087.46 2.722 295 423.30 1.060 200 416.89 1.044 199
in DMSO-d6
KBr disc
nujol mull
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