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3-(三氟甲氧基)苯乙酮

产品名称 3-(三氟甲氧基)苯乙酮

CAS号170141-63-6

分子式C9H7F3O2

分子量204.15


  • Mass

    MS-IW-8158          
    3'-(trifluoromethoxy)acetophenone
    C9H7F3O2            (Mass of molecular ion:    204)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          38.0       1.6
          39.0       1.3
          43.0      17.8
          50.0       2.2
          51.0       1.4
          62.0       1.4
          63.0       5.1
          64.0       5.4
          65.0       1.4
          69.0       5.0
          74.0       1.0
          75.0       4.1
          76.0       1.4
          77.0       1.4
          91.0       1.8
          92.0       4.9
          95.0      37.6
          96.0       2.7
         119.0       4.3
         161.0      28.3
         162.0       2.8
         189.0     100.0
         190.0       8.8
         191.0       1.0
         204.0      27.3
         205.0       2.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H7 F3 O2 0.05 ml : 0.5 ml CDCl3
    3'-(trifluoromethoxy)acetophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.890 B 7.805 C 7.515 D 7.422 E 2.615

         Hz     ppm     Int.
    

       3158.81   7.904     71
       3157.35   7.901     91
       3156.13   7.898     76
       3151.12   7.885     78
       3149.54   7.881    102
       3148.44   7.878     85
       3120.24   7.808     95
       3119.26   7.805    106
       3118.90   7.805    105
       3117.92   7.802     95
       3012.45   7.538     84
       3012.08   7.537     84
       3004.27   7.518    179
       2996.46   7.498    113
       2996.09   7.497    111
       2971.56   7.436     51
       2970.58   7.433     76
       2969.48   7.431     71
       2968.14   7.427     72
       2967.16   7.425     51
       2963.38   7.415     35
       2962.40   7.413     51
       2961.30   7.410     47
       2959.96   7.407     49
       2958.98   7.404     34
       1045.29   2.616   1000
       1041.99   2.608     42
    

in CDCl3



liquid film