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MassMS-NW-7584 1,2,3,4-tetrahydro-9-acridinamine hydrochloride C13H14N2 HCl (H2O) (Mass of molecular ion: 198)
Source Temperature: 160 °C Sample Temperature: 130 °C Direct, 75 eV
27.0 1.4 28.0 1.2 35.0 1.8 36.0 6.0 38.0 2.1 39.0 2.5 41.0 1.2 50.0 1.5 51.0 3.1 52.0 2.1 63.0 2.0 64.0 1.0 65.0 1.8 75.0 2.0 76.0 3.1 77.0 5.7 78.0 1.7 79.0 1.5 83.5 1.0 89.0 1.6 90.0 1.5 91.0 5.8 91.5 2.1 97.5 2.0 98.0 2.5 99.0 2.6 101.0 1.5 102.0 4.5 103.0 2.9 104.0 1.5 115.0 3.3 116.0 2.4 117.0 1.3 127.0 1.8 128.0 3.3 129.0 3.7 130.0 3.0 140.0 1.8 142.0 1.2 143.0 1.8 144.0 2.8 152.0 1.4 153.0 1.0 154.0 1.8 155.0 3.0 158.0 1.1 166.0 1.0 167.0 2.4 168.0 2.3 169.0 11.0 170.0 13.1 171.0 3.0 172.0 1.1 180.0 5.5 181.0 6.4 182.0 13.9 183.0 7.9 184.0 1.0 195.0 7.3 196.0 3.0 197.0 62.5 198.0 100.0 199.0 14.4 200.0 1.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H14 N2 0.039 g : 0.5 ml DMSO-d6 1,2,3,4-tetrahydro-9-acridinamine hydrochloride 
Assign. Shift(ppm)
A 14.11 B *1 8.99 C 8.573 D *1 8.09 E 7.971 F 7.837 G 7.557 J 3.005 K 2.542 L 1.852 SIGNAL K OVERLAPPED BY THE SOLVENT SIGNAL.
Hz ppm Int.5638.48 14.109 622 3595.66 8.998 91 3430.48 8.584 537 3422.15 8.563 558 3231.97 8.088 91 3191.37 7.986 534 3190.73 7.984 558 3182.82 7.965 738 3182.18 7.963 729 3139.87 7.857 350 3139.02 7.855 369 3133.04 7.840 447 3131.97 7.837 557 3124.70 7.819 309 3123.63 7.816 313 3028.54 7.578 335 3027.69 7.576 361 3024.91 7.569 69 3020.42 7.558 545 3019.14 7.555 412 3013.16 7.540 304 3012.09 7.537 306 1206.46 3.019 384 1201.12 3.006 767 1016.28 2.543 775 1012.22 2.533 382 1010.51 2.529 405 742.98 1.860 1000 740.20 1.853 947 737.85 1.847 993 726.95 1.819 188
in DMSO-d6
KBr disc
nujol mull
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