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MassMS-NW-9025 tetraoctylammonium iodide C32H68IN (Mass of molecular ion: 593)
Source Temperature: 220 °C Sample Temperature: 150 °C Direct, 75 eV
27.0 1.3 29.0 2.6 39.0 1.1 41.0 7.0 42.0 1.7 43.0 12.7 44.0 3.2 55.0 4.0 56.0 1.3 57.0 14.6 58.0 5.6 69.0 2.2 70.0 1.1 71.0 11.6 84.0 1.4 98.0 1.7 112.0 2.9 113.0 2.4 126.0 1.1 142.0 1.6 154.0 2.4 156.0 12.5 157.0 1.4 240.0 1.5 252.0 3.8 254.0 100.0 255.0 19.2 256.0 1.7 280.0 2.8 352.0 2.9 353.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C32 H68 I N 0.035 g : 0.5 ml CDCl3 tetraoctylammonium iodide 
Assign. Shift(ppm)
A 3.356 B 1.690 C 1.41 D 1.37 E 1.27 F 0.881
Hz ppm Int.1349.85 3.378 143 1341.43 3.357 135 1333.01 3.336 147 689.70 1.726 39 682.86 1.709 91 682.37 1.708 91 682.01 1.707 90 675.90 1.692 122 668.21 1.672 99 659.91 1.652 45 579.59 1.451 34 573.97 1.437 82 573.61 1.436 82 565.92 1.417 141 557.86 1.396 163 557.50 1.395 163 554.93 1.389 161 552.37 1.383 174 546.02 1.367 147 541.87 1.356 128 536.99 1.344 123 530.15 1.327 133 529.91 1.326 133 528.08 1.322 141 520.26 1.302 262 509.03 1.274 523 496.70 1.243 74 491.70 1.231 38 491.21 1.230 38 359.25 0.899 289 352.42 0.882 1000 345.34 0.865 344
in CDCl3
KBr disc
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