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MassMS-NW-3500 propylcyclohexane C9H18 (Mass of molecular ion: 126)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 9.8 28.0 1.6 29.0 8.4 39.0 11.3 40.0 1.9 41.0 30.7 42.0 6.2 43.0 6.9 51.0 1.3 53.0 4.2 54.0 6.8 55.0 56.0 56.0 9.9 57.0 2.4 65.0 1.0 67.0 12.8 68.0 3.2 69.0 8.7 70.0 4.7 81.0 2.2 82.0 47.2 83.0 100.0 84.0 7.7 97.0 2.5 98.0 1.0 126.0 14.4 127.0 1.4
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C9 H18 0.05 ml : 0.5 ml CDCl3 propylcyclohexane 
Assign. Shift(ppm)
A 1.77 to 1.580 B 1.31 C 1.22 D 1.18 to 1.100 E 0.871 F 0.86
Hz ppm Int.682.01 1.707 164 680.91 1.704 178 677.98 1.697 170 674.68 1.689 137 673.58 1.686 134 670.53 1.678 200 668.09 1.672 216 666.38 1.668 171 664.79 1.664 165 663.09 1.660 143 661.87 1.657 127 659.30 1.650 92 656.37 1.643 52 654.66 1.639 45 653.81 1.636 45 652.83 1.634 42 650.88 1.629 51 649.05 1.625 57 647.58 1.621 53 646.12 1.617 40 645.39 1.615 38 644.41 1.613 36 540.41 1.353 30 539.18 1.350 31 532.84 1.334 87 531.86 1.331 91 530.03 1.327 32 529.30 1.325 35 528.93 1.324 35 525.51 1.315 140 524.54 1.313 179 521.97 1.307 65 517.21 1.295 210 515.14 1.289 65 514.65 1.288 63 510.01 1.277 153 509.28 1.275 108 507.93 1.271 47 506.84 1.269 43 503.17 1.260 78 501.95 1.256 68 498.41 1.248 43 495.48 1.240 86 493.90 1.236 85 493.04 1.234 90 491.46 1.230 115 488.28 1.222 97 485.35 1.215 81 484.86 1.214 81 481.93 1.206 134 480.10 1.202 142 479.25 1.200 140 478.76 1.198 139 477.78 1.196 145 475.46 1.190 97 470.09 1.177 151 468.14 1.172 257 467.04 1.169 314 464.84 1.164 86 462.89 1.159 165 460.82 1.154 155 459.59 1.150 251 458.37 1.147 196 456.30 1.142 131 454.10 1.137 95 452.15 1.132 205 449.46 1.125 43 446.53 1.118 99 444.82 1.114 84 443.73 1.111 38 359.99 0.901 77 355.22 0.889 555 347.78 0.871 1000 345.58 0.865 165 342.53 0.858 77 340.58 0.853 485 335.08 0.839 112 324.95 0.814 34
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1H NMR 89.56 MHz C9 H18 0.04 ml : 0.5 ml CDCl3 propylcyclohexane Assign. Shift(ppm)
A 1.84 to 1.53 B 1.53 to 0.60 C 0.87
Hz ppm Int.156.56 1.749 231 153.94 1.719 244 147.81 1.651 382 146.38 1.635 371 137.88 1.540 61 137.38 1.534 59 134.94 1.507 60 133.75 1.494 58 133.19 1.488 59 132.81 1.483 59 130.38 1.456 59 130.06 1.453 58 128.00 1.430 82 126.38 1.412 68 126.06 1.408 68 122.06 1.363 128 120.56 1.347 137 119.88 1.339 135 116.63 1.303 181 115.13 1.286 229 113.44 1.267 198 105.50 1.178 606 101.19 1.130 308 99.31 1.109 282 97.13 1.085 257 92.31 1.031 147 90.81 1.014 139 89.44 0.999 129 84.13 0.940 346 83.38 0.931 401 80.38 0.898 187 80.06 0.894 188 77.88 0.870 1000 71.50 0.799 242 70.50 0.788 258 65.69 0.734 57 65.25 0.729 56
in CDCl3
liquid film
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