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MassMS-NW-5246 1,1,2,2-tetrakis(allyloxy)ethane C14H22O4 (Mass of molecular ion: 254)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 2.4 28.0 2.7 29.0 2.5 31.0 2.2 39.0 10.9 40.0 1.6 41.0 100.0 42.0 4.5 43.0 3.7 54.0 1.0 55.0 5.6 57.0 6.5 67.0 1.6 69.0 1.4 71.0 2.5 79.0 2.4 81.0 49.1 82.0 3.5 87.0 1.0 99.0 2.5 127.0 26.9 128.0 2.3 140.0 1.9 185.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H22 O4 0.04 ml : 0.5 ml CDCl3 1,1,2,2-tetrakis(allyloxy)ethane 
Assign. Shift(ppm)
A 5.91 B 5.30 C 5.18 D 4.505 E 4.17
Hz ppm Int.551.63 6.160 74 546.06 6.098 144 541.50 6.047 109 540.69 6.038 97 536.00 5.985 185 534.38 5.967 141 530.69 5.926 122 528.81 5.905 248 526.25 5.876 35 524.25 5.854 194 523.44 5.845 171 521.94 5.828 30 521.19 5.820 37 520.44 5.812 49 518.75 5.793 316 516.31 5.765 40 515.31 5.754 39 513.50 5.734 201 484.56 5.411 161 483.06 5.394 338 482.38 5.387 320 480.94 5.371 488 479.50 5.354 247 477.38 5.331 37 477.06 5.327 34 473.19 5.284 45 472.75 5.279 49 472.19 5.273 40 470.00 5.248 241 468.69 5.234 437 467.44 5.220 376 466.63 5.211 353 465.75 5.201 331 464.38 5.186 256 463.75 5.179 272 462.25 5.162 158 460.06 5.137 206 458.69 5.122 298 457.88 5.113 194 457.38 5.107 208 456.63 5.099 256 455.38 5.085 135 403.50 4.506 1000 387.06 4.322 30 381.56 4.261 33 380.31 4.247 43 379.69 4.240 55 378.44 4.226 101 376.81 4.208 458 375.56 4.194 785 374.19 4.179 490 372.88 4.164 159 371.75 4.151 373 371.13 4.144 397 370.31 4.135 597 369.94 4.131 593 368.88 4.119 365 363.31 4.057 36 363.00 4.054 35 361.75 4.040 30
in CDCl3
liquid film
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