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溴乙基二甲基氯硅烷

产品名称 溴乙基二甲基氯硅烷

CAS号16532-02-8

分子式C3H8BrClSi

分子量187.54

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  • Mass

    MS-NW-4937          
    (bromomethyl)chlorodimethylsilane
    C3H8BrClSi          (Mass of molecular ion:    186)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       1.9
          28.0       1.6
          29.0       3.1
          42.0       1.8
          43.0       4.1
          53.0       1.2
          63.0       9.0
          64.0       1.0
          65.0       9.0
          67.0       2.5
          77.0       1.4
          78.0       1.0
          79.0       2.3
          92.0       2.9
          93.0     100.0
          94.0       8.3
          95.0      35.0
          96.0       2.6
          97.0       1.1
         107.0       1.6
         109.0       1.9
         123.0       4.9
         124.0       1.0
         125.0       4.8
         143.0      10.9
         144.0       1.5
         145.0      13.7
         147.5       3.9
         152.0       1.8
         153.5       2.0
         157.0       1.3
         159.0       1.5
         171.0       4.9
         173.0       6.1
         175.0       1.7
         186.0       4.8
         188.0       6.3
         190.0       1.7
         197.0       2.4
         199.0       2.5
         225.0       2.3
         227.0       2.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C3 H8 Br Cl Si 0.04 ml : 0.5 ml CDCl3
    (bromomethyl)chlorodimethylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.638 B 0.572 J(A,SI-29)=4.3HZ J(B,SI-29)=7.3HZ

         Hz     ppm     Int.
    

        236.31   2.639    297
         54.81   0.612     47
         51.25   0.573   1000
         49.31   0.551     63
         47.69   0.533     51
    

in CDCl3



liquid film