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MassMS-IW-3732 o-phenylene phosphorochloridite C6H4ClO2P (Mass of molecular ion: 174)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 1.6 37.0 1.1 38.0 3.4 39.0 1.2 47.0 5.3 50.0 3.3 51.0 3.5 52.0 4.2 53.0 1.6 57.0 1.0 62.0 2.3 63.0 10.5 64.0 7.9 66.0 1.4 69.5 1.9 83.0 1.8 92.0 27.8 93.0 1.9 139.0 100.0 140.0 6.8 174.0 34.4 175.0 2.3 176.0 11.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 Cl O2 P 0.05 ml : 0.5 ml CDCl3 o-phenylene phosphorochloridite 
Assign. Shift(ppm)
A 7.219 B 7.096 J(A,P-31)=0.8HZ
Hz ppm Int.2895.51 7.246 50 2894.65 7.243 86 2893.68 7.241 63 2890.87 7.234 538 2889.89 7.232 504 2887.45 7.225 574 2886.47 7.223 540 2884.64 7.218 489 2884.16 7.217 441 2883.79 7.216 430 2881.47 7.210 693 2880.62 7.208 678 2877.44 7.200 123 2876.95 7.199 130 2876.59 7.198 128 2876.10 7.197 104 2844.73 7.119 152 2844.36 7.118 159 2840.33 7.108 1000 2836.91 7.099 688 2834.35 7.093 796 2830.93 7.084 785 2827.15 7.075 97 2826.29 7.072 80
in CDCl3
KBr disc
liquid film
nujol mull
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