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MS-NW-4000 ethylcyclopentane C7H14 (Mass of molecular ion: 98)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.0 26.0 1.4 27.0 13.7 28.0 2.6 29.0 12.5 38.0 1.2 39.0 18.6 40.0 3.5 41.0 63.7 42.0 41.3 43.0 7.0 50.0 1.0 51.0 1.7 53.0 5.1 54.0 5.3 55.0 47.9 56.0 44.7 57.0 7.4 65.0 1.2 67.0 10.0 68.0 66.4 69.0 100.0 70.0 56.1 71.0 3.2 83.0 8.2 98.0 12.3 99.0 1.0
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C7 H14 0.04 ml : 0.5 ml CDCl3 ethylcyclopentane Assign. Shift(ppm)
A 1.85 to 1.43 B 1.31 C 1.08 D 0.90 400MHZ : HSP-41-081
Hz ppm Int.
165.44 1.848 51 164.38 1.836 58 163.81 1.830 57 162.31 1.813 62 162.00 1.809 62 159.94 1.786 93 158.50 1.770 105 158.00 1.765 110 156.88 1.752 90 153.81 1.718 128 152.81 1.707 130 150.81 1.684 150 149.44 1.669 174 147.94 1.652 173 146.69 1.638 154 144.88 1.618 226 143.06 1.598 271 141.44 1.580 188 140.44 1.569 224 136.88 1.529 321 134.38 1.501 184 133.56 1.492 171 132.56 1.481 149 131.31 1.467 101 130.06 1.453 97 126.50 1.413 46 124.13 1.386 118 118.75 1.326 92 117.31 1.310 112 116.44 1.301 122 111.38 1.244 104 110.56 1.235 111 108.13 1.208 67 106.69 1.192 57 104.75 1.170 77 102.50 1.145 47 100.38 1.121 61 99.56 1.112 60 97.50 1.089 53 97.38 1.088 53 95.94 1.072 64 94.88 1.060 50 94.56 1.056 50 93.06 1.040 71 89.69 1.002 45 89.25 0.997 45 86.88 0.971 244 85.94 0.960 371 84.94 0.949 285 79.44 0.888 1000 78.50 0.877 304 76.94 0.860 130 73.13 0.817 115 71.81 0.802 166 69.81 0.780 98
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1H NMR 399.65 MHz C7 H14 0.05 ml : 0.5 ml CDCl3 ethylcyclopentane Assign. Shift(ppm)
A *1 1.72 B 1.67 C *2 1.58 D *2 1.50 E 1.310 F *1 1.073 G 0.888 90MHZ : HSP-03-882 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.
710.82 1.779 45 709.84 1.777 45 708.98 1.775 41 707.28 1.770 51 705.32 1.765 93 704.83 1.764 96 703.86 1.762 98 702.88 1.759 94 702.03 1.757 87 700.68 1.754 105 699.58 1.751 105 698.36 1.748 111 696.04 1.742 112 695.07 1.740 95 693.48 1.736 134 692.75 1.734 151 690.80 1.729 97 688.96 1.724 99 687.87 1.722 126 686.77 1.719 115 685.55 1.716 117 684.57 1.713 114 682.86 1.709 100 681.88 1.707 136 680.79 1.704 112 674.56 1.688 121 667.36 1.670 136 660.16 1.652 96 652.10 1.632 64 649.29 1.625 42 644.53 1.613 66 642.58 1.608 78 641.60 1.606 97 640.75 1.604 81 640.01 1.602 82 638.79 1.599 104 637.94 1.597 97 637.45 1.596 98 635.01 1.589 156 633.67 1.586 180 631.47 1.581 121 629.76 1.576 123 629.03 1.574 109 627.56 1.571 126 626.83 1.569 127 624.88 1.564 91 624.02 1.562 110 622.56 1.558 73 620.73 1.554 70 619.87 1.552 89 618.65 1.548 79 617.19 1.545 65 614.99 1.539 105 612.06 1.532 57 609.99 1.527 88 608.64 1.523 100 607.54 1.521 128 606.20 1.517 144 605.47 1.516 124 604.00 1.512 86 602.54 1.508 133 599.49 1.501 168 597.90 1.497 139 595.70 1.491 110 595.09 1.490 109 594.24 1.487 122 591.92 1.482 113 590.33 1.478 97 589.60 1.476 71 587.77 1.471 58 586.30 1.468 47 538.21 1.347 90 530.76 1.329 282 523.56 1.311 392 516.48 1.293 349 509.28 1.275 131 445.92 1.116 49 444.58 1.113 51 443.48 1.110 50 440.06 1.102 51 437.50 1.095 108 437.01 1.094 110 435.18 1.089 73 433.96 1.086 90 432.13 1.082 126 429.81 1.076 135 428.10 1.072 96 426.15 1.067 120 425.66 1.066 123 423.95 1.061 113 422.73 1.058 86 419.80 1.051 89 418.33 1.047 105 414.79 1.038 39 411.74 1.031 41 362.18 0.907 617 354.74 0.888 1000 347.29 0.869 550
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