二甲基氯甲基氧化膦

Mass

MS-IW-4076          
(chloromethyl)dimethylphosphine oxide
C3H8ClOP            (Mass of molecular ion:    126)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.6
      29.0       1.2
      31.0       1.0
      45.0       3.7
      46.0       2.1
      47.0      13.3
      48.0       1.0
      49.0      11.7
      57.0       1.3
      59.0       1.9
      61.0       2.1
      62.0       1.0
      63.0       1.2
      77.0     100.0
      78.0       3.2
      81.0       9.8
      83.0       4.6
     111.0       2.2
     126.0      19.6
     127.0       1.0
     128.0       6.3

Assign. Shift(ppm) A 3.597 B 1.656 J(A,P-31)=8.4HZ J(B,P-31)=3.2HZ

     Hz     ppm     Int.

   1441.77   3.608    310
   1433.35   3.587    311
    668.82   1.674    985
    668.46   1.673    992
    655.27   1.640   1000