双环戊烷

Mass

MS-IW-1708          
bicyclopentyl
C10H18              (Mass of molecular ion:    138)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      27.0       7.7
      28.0       1.1
      29.0       5.6
      39.0      14.8
      40.0       3.2
      41.0      55.6
      42.0       5.8
      43.0       5.2
      51.0       1.9
      52.0       1.2
      53.0       7.5
      54.0       9.1
      55.0      18.2
      56.0       2.1
      57.0       2.3
      65.0       4.0
      66.0      14.0
      67.0      97.8
      68.0     100.0
      69.0      51.0
      70.0       5.0
      71.0       9.7
      77.0       3.6
      78.0       1.2
      79.0       7.3
      80.0       3.6
      81.0      40.2
      82.0      63.6
      83.0      12.8
      91.0       3.1
      93.0       3.2
      94.0       4.0
      95.0      56.2
      96.0      54.0
      97.0       7.0
     104.0       2.8
     109.0      14.0
     110.0       6.8
     117.0       3.6
     123.0       1.0
     136.0       2.9
     138.0       9.4
     139.0       1.0
     146.0       2.0

Assign. Shift(ppm) A *1 1.724 B 1.61 to 1.55 C 1.49 D *1 1.122 ASSIGNED BY H-H COSY

     Hz     ppm     Int.

    704.10   1.762    230
    702.76   1.759    248
    701.29   1.755    241
    698.49   1.748    445
    697.39   1.746    455
    696.41   1.743    462
    695.56   1.741    429
    694.70   1.739    438
    693.12   1.735    537
    691.89   1.732    526
    689.45   1.726    489
    687.87   1.722    541
    686.89   1.719    560
    686.04   1.717    537
    684.69   1.714    486
    682.25   1.708    491
    680.91   1.704    481
    677.49   1.696    336
    675.29   1.690    306
    674.19   1.687    242
    670.29   1.678     69
    666.87   1.669     73
    665.77   1.666     70
    658.33   1.648     69
    655.88   1.642     64
    651.98   1.632    145
    650.63   1.628    148
    648.80   1.624    207
    647.34   1.620    148
    644.78   1.614    279
    643.80   1.611    305
    641.97   1.607    527
    640.99   1.604    508
    638.18   1.597    626
    634.40   1.588    819
    633.06   1.585   1000
    630.37   1.578    623
    629.15   1.575    643
    627.08   1.570    776
    626.10   1.567    827
    623.54   1.561    680
    621.70   1.556    613
    620.00   1.552    593
    619.38   1.550    615
    618.16   1.547    614
    617.19   1.545    520
    614.50   1.538    460
    612.55   1.533    668
    611.21   1.530    554
    608.15   1.522    398
    606.08   1.517    575
    603.76   1.511    655
    603.03   1.509    622
    602.17   1.507    642
    599.85   1.501    408
    598.14   1.497    756
    595.46   1.490    691
    594.36   1.488    639
    591.43   1.480    565
    590.70   1.479    529
    590.21   1.477    567
    588.87   1.474    442
    587.89   1.472    432
    586.43   1.468    413
    583.86   1.461    242
    583.13   1.460    245
    582.03   1.457    209
    580.81   1.454    164
    579.96   1.452    122
    578.13   1.447    138
    576.66   1.443     98
    575.81   1.441    101
    575.20   1.440     96
    574.46   1.438    114
    572.75   1.434     74
    471.31   1.180     68
    470.70   1.178     65
    465.33   1.165    217
    464.23   1.162    240
    463.26   1.160    220
    460.08   1.152    262
    457.40   1.145    481
    455.93   1.141    415
    454.83   1.139    346
    453.49   1.135    390
    451.54   1.130    488
    450.68   1.128    447
    449.22   1.125    554
    447.51   1.120    422
    445.19   1.114    503
    443.24   1.110    435
    442.02   1.107    394
    440.67   1.103    346
    438.72   1.098    348
    436.65   1.093    405
    432.01   1.081    138
    430.18   1.077    167
    428.96   1.074    152