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3-甲基碳酸胺

产品名称 3-甲基碳酸胺

CAS号16200-53-6

分子式C10H14O2

分子量166.22

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  • Mass

    MS-IW-8673          
    3-noradamantanecarboxylic acid
    C10H14O2            (Mass of molecular ion:    166)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.4
          27.0       4.0
          29.0       2.0
          39.0       8.0
          40.0       1.4
          41.0       9.4
          43.0       2.6
          45.0       1.3
          51.0       2.8
          52.0       1.5
          53.0       5.6
          54.0       4.7
          55.0       4.4
          65.0       3.6
          66.0       3.1
          67.0       8.1
          68.0       3.8
          69.0       1.3
          70.0       1.5
          73.0       1.6
          77.0      10.3
          78.0       6.7
          79.0      34.8
          80.0      41.3
          81.0     100.0
          82.0       7.8
          86.0       4.8
          87.0       7.8
          91.0       7.8
          92.0       5.7
          93.0       8.2
          94.0       3.1
          95.0       1.2
          97.0       2.0
          99.0       1.1
         105.0       3.8
         106.0       1.6
         107.0       1.3
         110.0       2.6
         111.0       1.5
         112.0       1.1
         119.0       1.4
         120.0       9.5
         121.0      17.0
         122.0       2.5
         123.0       5.5
         124.0       7.0
         125.0       2.4
         130.0       1.0
         133.0       1.2
         137.0       1.2
         138.0       1.0
         148.0       8.9
         149.0       1.5
         166.0      61.2
         167.0       7.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H14 O2 0.039 g : 0.5 ml CDCl3
    3-noradamantanecarboxylic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.714 B 2.306 C *1 2.094 D *2 1.82 E *1 1.81 F 1.63 G *2 1.59

         Hz     ppm     Int.
    

       1091.67   2.732    236
       1084.90   2.715    470
       1078.12   2.698    254
        921.14   2.305    709
        844.03   2.112    438
        842.93   2.110    449
        841.65   2.106    434
        839.82   2.102    294
        835.24   2.090    370
        833.41   2.086    553
        832.31   2.083    533
        831.03   2.080    502
        827.91   2.072    180
        734.13   1.837    271
        729.00   1.825    879
        726.07   1.817   1000
        722.77   1.809    400
        720.76   1.804    429
        718.75   1.799    790
        715.81   1.792    793
        658.85   1.649    844
        656.10   1.642    730
        650.42   1.628    240
        647.86   1.622    860
        645.84   1.617    904
        641.08   1.605    228
        640.35   1.603    220
        638.15   1.597    329
        637.42   1.595    365
        635.40   1.590    518
        633.21   1.585    338
        632.66   1.584    317
        622.40   1.558    164
    

in CDCl3



KBr disc



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