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网站主页CAS数据库列表 1619-34-7更多图谱奎宁环-3-醇(1619-34-7)红外图谱(IR2)

奎宁环-3-醇

产品名称 奎宁环-3-醇

CAS号1619-34-7

分子式C7H13NO

分子量127.18

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  • Mass

    MS-NW-2156          
    3-quinuclidinol
    C7H13NO             (Mass of molecular ion:    127)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       4.8
          18.0       2.6
          27.0       7.6
          28.0       3.9
          29.0       4.5
          30.0       8.4
          31.0       1.4
          39.0       5.5
          40.0       1.0
          41.0      11.7
          42.0     100.0
          43.0      28.3
          44.0       9.4
          53.0       2.5
          54.0       3.0
          55.0       9.2
          56.0       8.1
          57.0      10.4
          58.0      26.2
          59.0       1.0
          67.0       1.8
          68.0       3.9
          69.0       6.0
          70.0      12.9
          71.0       4.4
          72.0       2.8
          73.0       4.3
          80.0       1.1
          81.0       1.5
          82.0      11.0
          83.0       6.9
          84.0       4.7
          85.0       1.1
          86.0       2.5
          96.0       8.5
          97.0       1.9
          98.0      12.1
          99.0       5.2
         108.0       1.1
         109.0       1.0
         110.0       5.9
         112.0       6.8
         126.0       7.5
         127.0      37.8
         128.0       3.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H13 N O 0.036 g : 0.5 ml CDCl3
    3-quinuclidinol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.5 B 3.791 C *1 3.087 D *2 2.886 E *2 2.75 F *2 2.628 G *1 2.570 J *3 1.951 K 1.783 L *4 1.671 M *4 1.458 N *3 1.349 ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       1784.55   4.466    127
       1520.26   3.804    641
       1518.92   3.801    681
       1516.60   3.795    457
       1515.38   3.792    680
       1514.28   3.790    498
       1511.84   3.783    674
       1510.62   3.780    702
       1246.34   3.119    467
       1244.02   3.113    490
       1238.04   3.098    470
       1235.72   3.093    505
       1232.30   3.084    557
       1229.98   3.078    577
       1224.00   3.063    493
       1221.68   3.057    513
       1157.84   2.898    464
       1155.15   2.891    482
       1152.22   2.884    488
       1109.86   2.778    465
       1108.03   2.773    426
       1104.61   2.764    488
       1102.05   2.758    662
       1099.24   2.751    762
       1097.17   2.746    728
       1096.07   2.743    724
       1092.77   2.735    555
       1090.21   2.728    524
       1088.26   2.724    503
       1085.82   2.717    538
       1052.37   2.634    492
       1049.80   2.627    520
       1047.36   2.621    487
       1036.25   2.593    692
       1033.57   2.587    841
       1030.52   2.579    506
       1022.09   2.558    459
       1019.17   2.551    637
       1016.48   2.544    424
        784.06   1.962    367
        781.37   1.956    460
        778.56   1.949    462
        776.12   1.942    394
        717.65   1.796    546
        714.36   1.788    980
        711.18   1.780   1000
        708.01   1.772    585
        679.44   1.701    333
        674.32   1.688    335
        671.26   1.680    461
        669.19   1.675    379
        667.60   1.671    416
        666.26   1.668    506
        662.60   1.658    384
        661.25   1.655    398
        657.35   1.645    340
        656.13   1.642    368
        596.44   1.493    341
        593.63   1.486    348
        590.70   1.479    365
        586.06   1.467    513
        583.25   1.460    582
        580.32   1.453    561
        577.64   1.446    430
        535.77   1.341    385
        528.20   1.322    221
    

in CDCl3



KBr disc



nujol mull





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