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2,4,6-三甲基苯磺酰肼

产品名称 2,4,6-三甲基苯磺酰肼

CAS号16182-15-3

分子式C9H14N2O2S

分子量214.28

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  • Mass

    MS-IW-8196          
    2,4,6-trimethylbenzenesulfonohydrazide
    C9H14N2O2S          (Mass of molecular ion:    214)
    

       Source Temperature: 150 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          17.0       2.5
          18.0      11.0
          27.0       3.3
          28.0       9.1
          29.0       9.7
          30.0      10.4
          31.0       5.2
          39.0       6.7
          41.0       8.9
          45.0       3.2
          48.0       5.7
          50.0       2.1
          51.0       5.9
          52.0       2.2
          53.0       3.6
          57.5       1.7
          58.0       2.5
          59.0       3.3
          62.0       1.1
          63.0       3.5
          64.0      20.0
          65.0       6.3
          66.0       1.1
          74.0       1.2
          75.0       1.5
          76.0       1.3
          77.0      15.9
          78.0       5.4
          79.0      11.3
          80.0       1.0
          89.0       1.5
          91.0      29.5
          92.0       3.4
          93.0       3.8
         102.0       1.9
         103.0      10.7
         104.0       6.3
         105.0     100.0
         106.0      11.9
         107.0       3.7
         115.0       7.9
         116.0       2.0
         117.0      10.6
         118.0       3.1
         119.0      78.5
         120.0      84.4
         121.0      11.8
         134.0       2.5
         135.0      10.0
         136.0       4.6
         137.0       2.2
         139.0       4.0
         149.0       2.1
         150.0       1.8
         151.0       5.6
         152.0      14.8
         153.0       2.0
         165.0       2.6
         166.0       4.5
         167.0       4.3
         168.0       4.3
         183.0       1.2
         184.0      24.8
         185.0      23.2
         186.0       3.8
         187.0       1.3
         214.0       9.8
         215.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H14 N2 O2 S 0.037 g : 0.5 ml CDCl3
    2,4,6-trimethylbenzenesulfonohydrazide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.983 B 5.85 C 3.47 D 2.645 E 2.311

         Hz     ppm     Int.
    

       2791.02   6.984    249
       2790.65   6.983    249
       1388.31   3.474     24
       1057.25   2.646   1000
        923.58   2.311    501
    

in CDCl3



KBr disc



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