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网站主页CAS数据库列表 1611-56-9更多图谱11-溴-1-十一醇(1611-56-9)核磁图(1HNMR)

11-溴-1-十一醇

产品名称 11-溴-1-十一醇

CAS号1611-56-9

分子式C11H23BrO

分子量251.2

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  • Mass

    MS-IW-0764          
    11-bromo-1-undecanol
    C11H23BrO           (Mass of molecular ion:    250)
    

       Source Temperature: 180 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       3.5
          27.0       8.2
          28.0       1.5
          29.0      13.5
          31.0       9.0
          39.0       7.3
          40.0       1.5
          41.0      50.1
          42.0      13.9
          43.0      30.0
          44.0       2.5
          45.0       1.8
          53.0       3.8
          54.0       8.9
          55.0     100.0
          56.0      24.5
          57.0      21.0
          58.0       1.1
          67.0      17.8
          68.0      32.5
          69.0      97.0
          70.0      21.0
          71.0       7.2
          73.0       2.0
          79.0       1.4
          81.0      11.6
          82.0      25.1
          83.0      75.8
          84.0      10.3
          85.0       2.1
          87.0       1.5
          95.0       7.9
          96.0       6.1
          97.0      44.4
          98.0       5.5
         107.0       2.0
         109.0       4.2
         110.0       2.4
         111.0      10.9
         112.0       1.1
         121.0       1.3
         123.0       3.9
         124.0       2.1
         125.0       6.8
         134.0       2.8
         135.0      10.7
         136.0       3.0
         137.0      10.0
         148.0      27.9
         149.0       4.5
         150.0      27.1
         151.0       4.0
         162.0      20.3
         163.0       2.7
         164.0      19.5
         165.0       2.1
         176.0       2.0
         178.0       1.8
         190.0       1.2
         192.0       1.0
         204.0       3.7
         206.0       3.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C11 H23 Br O 0.042 g : 0.5 ml CDCl3
    11-bromo-1-undecanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.629 B 3.407 C 1.850 D 1.63 E 1.56 F 1.42 G 1.34 J 1.32 K 1.28

         Hz     ppm     Int.
    

       1457.15   3.647    150
       1450.56   3.630    291
       1443.85   3.613    155
       1368.77   3.425    307
       1361.94   3.408    624
       1355.10   3.391    326
        754.27   1.888     70
        747.31   1.870    183
        740.23   1.853    198
        732.54   1.833    191
        725.71   1.816     81
        653.32   1.635    164
        637.70   1.596     33
        630.98   1.579     96
        623.66   1.561    137
        616.46   1.543    127
        609.74   1.526     51
        574.95   1.439     78
        572.27   1.432     67
        567.87   1.421    108
        560.55   1.403     88
        553.47   1.385     51
        550.78   1.379     36
        538.82   1.349    110
        534.06   1.337    135
        533.08   1.334    133
        525.39   1.315    257
        524.41   1.313    258
        512.82   1.284   1000
    

in CDCl3



KBr disc



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