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MS-IW-0063 2-piperidinimine hydrochloride C5H10N2 HCl (Mass of molecular ion: 98)
Source Temperature: 210 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 1.5 18.0 3.4 26.0 1.0 27.0 4.4 28.0 10.1 29.0 2.8 30.0 26.3 35.0 3.8 36.0 49.3 37.0 1.4 38.0 16.3 39.0 5.0 40.0 1.7 41.0 18.4 42.0 34.5 43.0 50.3 44.0 8.4 48.0 1.2 52.0 1.1 53.0 1.8 54.0 7.8 55.0 8.0 56.0 7.6 57.0 2.3 68.0 1.5 69.0 1.7 70.0 68.8 71.0 3.2 80.0 1.2 83.0 1.5 84.0 2.5 97.0 14.6 98.0 100.0 99.0 10.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C5 H10 N2 0.031 g : 0.5 ml DMSO-d6 2-piperidinimine hydrochloride Assign. Shift(ppm)
A *1 9.79 B *1 8.92 C *1 8.58 D 3.27 E 2.55 F 1.70
Hz ppm Int.
3914.18 9.795 220 3565.98 8.923 219 3429.11 8.581 231 1308.75 3.275 532 1306.92 3.271 517 1024.17 2.563 307 1018.07 2.548 688 999.15 2.501 55 997.16 2.496 41 692.44 1.733 86 689.54 1.726 136 680.69 1.704 921 677.49 1.696 1000 674.29 1.688 957 664.52 1.663 145 661.93 1.657 96 659.79 1.651 59
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