二硝散

Mass

MS-NW-2415          
2,4-dinitrophenyl thiocyanate
C7H3N3O4S           (Mass of molecular ion:    225)

   Source Temperature: 210 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.3
      18.0       6.7
      26.0       1.1
      27.0       1.7
      28.0       5.4
      29.0       1.5
      30.0     100.0
      32.0       1.3
      37.0       4.5
      38.0       6.8
      39.0       5.1
      43.0       2.2
      44.0       2.4
      45.0      16.7
      46.0       3.6
      48.0       1.3
      49.0       1.5
      50.0       5.4
      51.0       7.2
      52.0       2.9
      53.0       3.3
      57.0       3.7
      58.0       6.3
      60.0       1.0
      61.0       6.6
      62.0      16.7
      63.0      38.2
      64.0       6.8
      65.0       1.5
      68.0       1.1
      69.0      45.7
      70.0       9.2
      71.0       2.8
      73.0       3.5
      74.0      24.9
      75.0      25.7
      76.0       6.7
      77.0       5.5
      78.0       2.1
      79.0      22.8
      80.0       3.0
      81.0       5.3
      82.0      18.0
      83.0       7.0
      84.0       1.5
      85.0       1.0
      86.0       1.1
      87.0       1.4
      88.0      24.4
      89.0       5.4
      91.0      14.2
      92.0       1.5
      93.0       5.9
      94.0      13.4
      95.0      10.4
      96.0       2.6
      97.0       1.0
      98.0       1.0
     101.0       1.3
     103.0      10.5
     104.0       7.2
     105.0       3.5
     106.0       9.3
     107.0      15.4
     108.0       1.9
     109.0       4.0
     114.0       3.0
     115.0      29.7
     116.0       3.2
     120.0       3.1
     121.0      10.2
     122.0       2.5
     123.0       2.7
     131.0      23.5
     132.0       5.1
     133.0      16.6
     134.0       2.0
     135.0       1.0
     136.0       1.4
     137.0       5.7
     149.0       5.1
     151.0       4.2
     152.0       3.8
     161.0       6.0
     179.0       5.2
     183.0       6.1
     195.0       1.7
     209.0       1.7
     225.0      46.3
     226.0       4.5
     227.0       2.5

Assign. Shift(ppm) A 9.220 B 8.620 C 8.311

     Hz     ppm     Int.

    827.19   9.237    584
    826.88   9.233    568
    824.81   9.210    672
    824.44   9.206    634
    778.88   8.697    471
    776.44   8.670    407
    769.94   8.597    792
    767.50   8.570    745
    747.75   8.350   1000
    747.38   8.346    921
    738.88   8.251    565
    738.44   8.246    524