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MS-NW-4815 ethyl isonicotinate C8H9NO2 (Mass of molecular ion: 151)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.6 18.0 1.8 26.0 2.7 27.0 8.2 28.0 2.6 29.0 21.8 38.0 1.0 39.0 1.8 45.0 11.6 49.0 1.4 50.0 12.7 51.0 41.6 52.0 7.9 53.0 1.1 76.0 1.2 77.0 2.3 78.0 61.6 79.0 14.3 80.0 1.2 105.0 3.5 106.0 100.0 107.0 9.7 108.0 1.0 123.0 59.5 124.0 5.4 133.0 4.0 136.0 1.0 137.0 4.4 150.0 1.6 151.0 36.7 152.0 3.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O2 0.04 ml : 0.5 ml CDCl3 ethyl isonicotinate Assign. Shift(ppm)
A 8.774 B 7.848 C 4.418 D 1.415
Hz ppm Int.
789.00 8.810 396 787.38 8.792 209 784.63 8.761 231 783.00 8.743 454 705.81 7.881 560 704.19 7.863 294 702.63 7.846 29 701.44 7.833 248 699.81 7.814 497 406.69 4.541 124 399.50 4.461 467 392.38 4.382 489 385.31 4.303 146 133.69 1.493 482 126.69 1.415 1000 124.44 1.390 31 119.44 1.334 427
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