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网站主页CAS数据库列表 1569-69-3更多图谱环己硫醇(1569-69-3)核磁图(1HNMR)

环己硫醇

产品名称 环己硫醇

CAS号1569-69-3

分子式C6H12S

分子量116.22

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  • Mass

    MS-NW-3999          
    cyclohexanethiol
    C6H12S              (Mass of molecular ion:    116)
    

       Source Temperature: 300 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       1.4
          27.0      13.5
          28.0       3.7
          29.0       9.2
          32.0       1.0
          38.0       1.2
          39.0      17.8
          40.0       2.1
          41.0      54.3
          42.0       3.5
          43.0       4.8
          45.0      10.0
          46.0       1.4
          47.0       6.7
          50.0       1.7
          51.0       2.8
          52.0       1.2
          53.0       8.5
          54.0      29.2
          55.0     100.0
          56.0       5.6
          58.0       2.6
          59.0       4.2
          60.0       9.5
          61.0       3.2
          65.0       1.6
          66.0       1.3
          67.0      66.6
          68.0       4.6
          69.0       2.2
          71.0       1.6
          73.0       8.5
          74.0       1.8
          77.0       1.8
          79.0       3.5
          81.0      10.3
          82.0      57.1
          83.0      76.4
          84.0       5.5
          87.0       1.6
         116.0      42.0
         117.0       3.5
         118.0       2.2
         148.0       3.1
         230.0       1.3
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H12 S 0.04 ml : 0.5 ml CDCl3
    cyclohexanethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.793 B 2.01 C 1.75 D 1.61 E 1.51 F 1.34 G 1.31 J 1.22 ASSIGNED BY COSY.

         Hz     ppm     Int.
    

       1129.15   2.826     47
       1125.49   2.817     60
       1122.68   2.810     80
       1118.90   2.800    110
       1115.23   2.791     92
       1112.18   2.783     97
       1108.40   2.774     89
       1104.74   2.765     46
       1101.81   2.757     39
        810.18   2.028    126
        808.84   2.024    141
        807.62   2.021    158
        806.52   2.019    176
        805.42   2.016    202
        804.69   2.014    206
        799.32   2.001    175
        798.22   1.998    153
        794.19   1.988    295
        719.48   1.801     32
        718.38   1.798     36
        717.41   1.796     37
        716.67   1.794     36
        715.58   1.791     40
        714.11   1.787     41
        713.13   1.785     41
        712.89   1.784     41
        707.28   1.770    141
        704.22   1.763    232
        703.74   1.761    231
        703.00   1.760    216
        701.78   1.756    198
        699.83   1.752    233
        695.56   1.741    176
        694.46   1.738    184
        691.77   1.731    181
        690.80   1.729    180
        689.33   1.725    150
        687.99   1.722    137
        684.08   1.712     48
        653.56   1.636     74
        652.34   1.633     97
        650.88   1.629    102
        649.54   1.626    109
        648.68   1.624    124
        647.34   1.620    105
        645.63   1.616     89
        644.29   1.613     87
        643.31   1.610     93
        641.85   1.607     85
        640.14   1.602     90
        639.16   1.600     95
        637.82   1.596    117
        636.47   1.593    110
        633.42   1.585     81
        632.20   1.582     63
        605.10   1.515   1000
        602.05   1.507     32
        598.51   1.498    953
        558.47   1.398     88
        556.15   1.392     73
        547.12   1.369    213
        544.56   1.363    201
        535.64   1.341    440
        527.71   1.321    251
        526.86   1.319    244
        524.90   1.314    442
        518.55   1.298     70
        515.75   1.291    165
        513.06   1.284    232
        510.38   1.278    155
        509.64   1.276    132
        506.59   1.268     42
        503.78   1.261     80
        500.98   1.254    139
        498.78   1.249    117
        498.05   1.247    121
        496.46   1.243     78
        495.12   1.239     65
        493.29   1.235     58
        488.40   1.223     91
        485.47   1.215     93
        482.79   1.209     70
        476.93   1.194     69
        473.88   1.186     69
        470.58   1.178     38
    


  • 1H NMR 89.56 MHz
    C6 H12 S 0.04 ml : 0.5 ml CDCl3
    cyclohexanethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.78 B 1.98 C 1.70 D 1.70 to 1.03 E 1.493

         Hz     ppm     Int.
    

        257.75   2.878     37
        257.63   2.877     37
        257.06   2.871     37
        256.50   2.865     37
        255.00   2.848     41
        254.00   2.837     51
        250.94   2.802     53
        249.56   2.787     52
        248.81   2.779     50
        247.13   2.760     54
        244.94   2.735     47
        244.38   2.729     47
        243.13   2.715     49
        241.81   2.700     36
        241.31   2.695     35
        240.31   2.684     36
        239.50   2.675     31
        187.88   2.098     61
        186.75   2.086     51
        183.56   2.050     96
        182.13   2.034     95
        177.63   1.984    157
        176.88   1.975    165
        174.69   1.951    125
        173.19   1.934    107
        172.06   1.922     99
        170.94   1.909     96
        165.81   1.852     72
        164.75   1.840     75
        162.94   1.820     91
        160.25   1.790    136
        159.38   1.780    144
        159.25   1.779    144
        158.31   1.768    149
        155.81   1.740    164
        153.94   1.719    133
        152.50   1.703    121
        151.13   1.688    116
        150.69   1.683    115
        150.00   1.675    117
        149.88   1.674    117
        148.88   1.663    114
        148.19   1.655    118
        147.38   1.646    117
        147.06   1.643    117
        146.69   1.638    118
        144.50   1.614    144
        142.19   1.588    109
        140.94   1.574    105
        140.06   1.564    102
        139.44   1.557    107
        138.81   1.550    108
        136.94   1.530   1000
        135.00   1.508    123
        134.25   1.499    114
        133.00   1.486    106
        132.44   1.479    113
        130.44   1.457    907
        127.81   1.428    235
        124.06   1.386    139
        118.06   1.319    365
        117.00   1.307    337
        112.88   1.261    204
        110.50   1.234    256
        109.69   1.225    276
        105.81   1.182     81
        104.56   1.168     63
        103.25   1.153     68
        100.31   1.121     34
         99.94   1.116     32
    

in CDCl3



liquid film