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MassMS-IW-4054 2,2-dimethyl-2,3-dihydro-7-benzofuranol C10H12O2 (Mass of molecular ion: 164)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 3.4 28.0 1.5 29.0 1.6 39.0 9.8 40.0 2.1 41.0 7.0 43.0 3.8 50.0 2.0 51.0 9.6 52.0 3.5 53.0 3.8 55.0 5.6 56.0 1.0 63.0 2.7 64.0 1.4 65.0 6.5 66.0 3.8 67.0 2.2 73.5 1.0 74.0 1.1 74.5 1.5 77.0 13.9 78.0 6.1 79.0 4.2 80.0 1.2 81.0 1.5 82.0 1.8 89.0 1.3 91.0 10.9 92.0 1.9 93.0 3.8 94.0 5.1 95.0 3.3 102.0 1.4 103.0 16.8 104.0 1.9 105.0 3.7 106.0 2.1 107.0 8.3 108.0 1.5 110.0 5.2 115.0 3.5 116.0 1.2 117.0 8.0 118.0 4.7 119.0 2.7 120.0 1.0 121.0 21.3 122.0 27.9 123.0 28.8 124.0 5.8 127.0 1.6 131.0 31.5 132.0 3.9 134.0 1.1 135.0 6.1 136.0 3.0 137.0 1.3 145.0 7.6 146.0 6.9 147.0 13.2 148.0 3.0 149.0 82.9 150.0 8.3 163.0 4.9 164.0 100.0 165.0 11.0 166.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H12 O2 0.05 ml : 0.5 ml CDCl3 2,2-dimethyl-2,3-dihydro-7-benzofuranol 
Assign. Shift(ppm)
A 6.74 B 6.69 C 5.85 D 3.007 E 1.468
Hz ppm Int.2698.97 6.754 41 2695.92 6.746 68 2693.73 6.741 38 2692.75 6.738 71 2691.77 6.736 47 2689.58 6.730 121 2686.04 6.721 93 2678.96 6.704 254 2675.78 6.696 141 2672.61 6.688 233 2669.43 6.680 22 2668.70 6.678 29 2337.65 5.850 316 1201.78 3.008 410 586.79 1.469 1000 576.42 1.443 26
in CDCl3
liquid film
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