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MassMS-NW-8051 2-(3,4-dihydroxyphenyl)valeramide C11H15NO3 (Mass of molecular ion: 209)
Source Temperature: 220 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 1.6 27.0 2.3 28.0 2.2 29.0 1.6 39.0 3.0 41.0 1.6 44.0 3.1 51.0 3.1 53.0 1.7 55.0 4.4 63.0 1.5 65.0 3.2 66.0 1.0 77.0 5.7 78.0 1.0 79.0 1.1 89.0 2.1 90.0 1.1 91.0 3.2 93.0 1.3 94.0 1.3 103.0 1.1 105.0 1.4 107.0 1.0 110.0 1.0 115.0 1.0 119.0 1.1 122.0 2.5 123.0 100.0 124.0 8.2 135.0 1.1 136.0 4.2 137.0 1.5 138.0 1.9 147.0 1.4 150.0 1.8 165.0 28.4 166.0 4.3 167.0 10.8 168.0 1.0 171.0 1.0 209.0 16.5 210.0 2.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H15 N O3 0.023 g : 0.5 ml DMSO-d6 2-(3,4-dihydroxyphenyl)valeramide 
Assign. Shift(ppm)
A *1 8.73 B *1 8.65 C *2 7.28 D 6.736 E *2 6.69 F 6.615 G 6.537 J 3.207 K *3 1.804 L *3 1.458 M 1.172 N 0.852
Hz ppm Int.3488.89 8.730 46 3455.69 8.647 46 2911.99 7.287 158 2693.12 6.739 373 2691.04 6.734 399 2674.19 6.692 162 2649.05 6.629 344 2640.99 6.609 553 2616.94 6.549 238 2614.87 6.543 232 2608.76 6.528 152 2606.69 6.523 150 1289.79 3.228 97 1282.84 3.210 138 1281.49 3.207 139 1274.54 3.190 105 733.64 1.836 34 730.96 1.830 61 726.44 1.818 50 724.98 1.815 68 722.29 1.808 52 720.70 1.804 49 717.65 1.796 77 711.91 1.782 65 708.98 1.775 47 703.13 1.760 35 593.38 1.485 63 590.82 1.479 44 586.79 1.469 73 584.35 1.463 76 580.20 1.452 65 577.88 1.446 77 573.49 1.435 42 571.41 1.430 63 564.82 1.414 33 347.53 0.870 476 340.21 0.852 1000 332.76 0.833 382
in DMSO-d6
KBr disc
nujol mull
