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1,2-二(1-萘基)乙烷

产品名称 1,2-二(1-萘基)乙烷

CAS号15374-45-5

分子式C22H18

分子量282.38

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  • Mass

    MS-IW-3984          
    1,1'-ethylenedinaphthalene
    C22H18              (Mass of molecular ion:    282)
    

       Source Temperature: 160 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

         115.0       8.9
         139.0       2.5
         141.0     100.0
         142.0      12.4
         153.0       1.0
         282.0      25.7
         283.0       6.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C22 H18 0.045 g : 0.5 ml CDCl3
    1,1'-ethylenedinaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.105 B 7.864 C 7.727 D 7.51 E 7.48 F 7.378 G 7.327 J 3.496 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       3244.26   8.118    128
       3243.16   8.116    149
       3234.74   8.094    156
       3147.71   7.877    143
       3145.63   7.871    106
       3140.14   7.858    178
       3138.31   7.853    157
       3092.29   7.738    165
       3084.23   7.718    185
       3009.52   7.531     60
       3007.93   7.527     78
       3002.81   7.514    161
       3001.22   7.510    152
       2999.76   7.506     77
       2995.00   7.495    315
       2992.92   7.489    301
       2988.04   7.477     82
       2987.06   7.475    146
       2985.60   7.471    160
       2980.22   7.458     68
       2978.88   7.454     59
       2957.15   7.400    139
       2950.07   7.382    248
       2942.02   7.362    230
       2930.91   7.334    216
       2929.81   7.331    235
       2923.95   7.317    124
       2922.85   7.314    121
       1397.22   3.497   1000
    

in CDCl3



KBr disc



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