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MS-NW-1956 diethylammonium diethyldithiocarbamate C5H11NS2 C4H11N (Mass of molecular ion: 222)
Source Temperature: 230 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.1 18.0 6.8 26.0 2.0 27.0 11.0 28.0 13.4 29.0 14.7 30.0 79.7 31.0 1.1 32.0 6.0 38.0 3.2 40.0 1.1 41.0 2.7 42.0 8.7 43.0 2.2 44.0 26.4 56.0 5.5 57.0 1.3 58.0 100.0 59.0 3.8 72.0 14.6 73.0 25.3 74.0 1.3 76.0 83.4 77.0 2.2 78.0 7.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H22 N2 S2 0.048 g : 0.5 ml CDCl3 diethylammonium diethyldithiocarbamate Assign. Shift(ppm)
A 8.93 B 4.097 C 3.196 D 1.396 E 1.265
Hz ppm Int.
799.94 8.932 344 377.94 4.220 84 370.81 4.141 297 363.81 4.063 314 356.75 3.984 97 297.94 3.327 102 290.44 3.243 407 283.13 3.162 440 275.88 3.081 133 132.00 1.474 443 124.88 1.395 1000 120.00 1.340 374 117.38 1.311 391 113.06 1.263 871 105.88 1.183 318
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