环癸酮

Mass

MS-NW-6419          
cyclodecanone
C10H18O             (Mass of molecular ion:    154)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.0
      18.0       3.6
      26.0       2.7
      27.0      35.1
      28.0      14.2
      29.0      34.6
      31.0       1.4
      38.0       1.4
      39.0      31.2
      40.0       7.4
      41.0      99.2
      42.0      46.9
      43.0      33.8
      44.0       1.8
      45.0       1.4
      50.0       1.3
      51.0       2.4
      52.0       1.3
      53.0       9.1
      54.0      19.4
      55.0     100.0
      56.0      47.6
      57.0      14.3
      58.0      49.5
      59.0      12.1
      65.0       1.7
      66.0       2.3
      67.0      21.4
      68.0      18.3
      69.0      37.8
      70.0      27.8
      71.0      30.0
      72.0       5.3
      77.0       2.0
      79.0       9.6
      80.0       6.2
      81.0      20.4
      82.0      13.9
      83.0      32.1
      84.0      42.6
      85.0       6.1
      86.0       2.2
      91.0       1.2
      93.0       8.0
      94.0      18.1
      95.0       8.9
      96.0      22.3
      97.0      50.9
      98.0      70.9
      99.0       7.0
     100.0       1.1
     107.0       7.0
     108.0       2.5
     110.0       3.2
     111.0      79.1
     112.0      25.1
     113.0       3.7
     121.0       3.3
     125.0      15.5
     126.0       2.1
     136.0       1.8
     139.0       1.6
     154.0      26.5
     155.0       3.2

Assign. Shift(ppm) A 2.522 B 1.854 C 1.496 D 1.36

     Hz     ppm     Int.

   1014.53   2.539    869
   1010.62   2.529    300
   1008.30   2.523    588
   1005.98   2.518    249
   1005.13   2.516    245
   1001.95   2.508    904
    753.30   1.885    259
    749.51   1.876    207
    747.44   1.871    342
    744.75   1.864    337
    741.09   1.855    531
    738.40   1.848    197
    737.30   1.845    307
    734.86   1.839    354
    732.54   1.833    185
    728.76   1.824    254
    610.23   1.527    119
    606.20   1.517    167
    603.88   1.512    274
    601.56   1.506    284
    597.90   1.497    368
    595.58   1.491    250
    594.85   1.489    255
    592.04   1.482    266
    589.60   1.476    167
    586.18   1.467    123
    549.80   1.376    140
    546.63   1.368    465
    545.04   1.364    663
    543.46   1.360    804
    541.99   1.357   1000
    538.57   1.348    401
    534.67   1.338    216