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MS-NW-9639 tris(2-methoxyethyl) borate C9H21BO6 (Mass of molecular ion: 236)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 5.5 27.0 1.8 28.0 2.8 29.0 8.9 31.0 10.6 42.0 1.7 43.0 6.0 44.0 1.4 45.0 51.2 46.0 1.8 47.0 3.6 58.0 13.0 59.0 30.3 71.0 1.0 72.0 17.7 73.0 67.0 74.0 1.7 76.0 2.2 85.0 1.1 86.0 1.7 87.0 3.7 101.0 1.5 102.0 2.3 103.0 8.5 115.0 2.3 116.0 9.4 117.0 35.8 118.0 1.6 129.0 1.4 130.0 5.2 160.0 27.5 161.0 100.0 162.0 7.0 163.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H21 B O6 0.05 ml : 0.5 ml CDCl3 tris(2-methoxyethyl) borate Assign. Shift(ppm)
A 3.948 B 3.492 C 3.373
Hz ppm Int.
359.00 4.009 77 354.75 3.962 141 353.25 3.945 84 352.19 3.933 53 349.31 3.901 127 317.56 3.546 144 314.88 3.516 57 313.81 3.504 88 312.25 3.487 158 308.00 3.440 86 307.56 3.435 91 302.19 3.375 1000