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MS-NW-7963 2-methyl-2-phenylsuccinimide C11H11NO2 (Mass of molecular ion: 189)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.5 39.0 5.3 41.0 1.1 50.0 3.3 51.0 8.4 52.0 1.9 57.0 1.1 57.5 3.4 58.0 9.1 58.5 1.0 59.0 1.1 63.0 2.7 65.0 2.3 70.0 1.0 73.0 1.2 74.0 1.3 75.0 1.2 76.0 1.6 77.0 10.6 78.0 11.2 89.0 1.3 91.0 6.8 102.0 2.5 103.0 16.0 104.0 1.7 115.0 5.7 116.0 1.7 117.0 29.3 118.0 100.0 119.0 10.4 189.0 24.6 190.0 3.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H11 N O2 0.042 g : 0.5 ml CDCl3 2-methyl-2-phenylsuccinimide Assign. Shift(ppm)
A 9.2 B 7.37 to 7.33 C *1 3.107 D *1 2.904 E 1.729 J(C,D)=-18.4HZ
Hz ppm Int.
824.63 9.208 33 667.81 7.457 25 666.31 7.440 44 664.63 7.422 105 663.75 7.412 78 661.19 7.383 247 658.44 7.352 879 655.44 7.319 202 653.00 7.292 109 651.31 7.273 82 647.44 7.230 40 646.94 7.224 38 292.94 3.271 85 274.56 3.066 330 263.94 2.948 365 245.56 2.742 95 160.50 1.793 35 154.94 1.731 1000 149.88 1.674 29
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