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MassMS-NW-3494 cis-3-octene C8H16 (Mass of molecular ion: 112)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.6 26.0 1.9 27.0 25.0 28.0 3.9 29.0 18.8 38.0 1.9 39.0 26.0 40.0 5.0 41.0 100.0 42.0 37.5 43.0 17.7 50.0 2.0 51.0 3.7 52.0 1.8 53.0 11.1 54.0 7.5 55.0 95.4 56.0 53.5 57.0 16.4 58.0 1.2 63.0 1.1 65.0 2.3 66.0 1.1 67.0 10.3 68.0 6.6 69.0 47.1 70.0 48.4 71.0 6.4 77.0 1.6 79.0 1.7 81.0 2.7 82.0 2.0 83.0 24.1 84.0 7.4 85.0 1.5 97.0 1.9 112.0 35.8 113.0 3.4
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C8 H16 0.05 ml : 0.5 ml CDCl3 cis-3-octene 
Assign. Shift(ppm)
A *1 5.35 B *1 5.32 C 2.05 D 2.02 E 1.34 F 1.31 G 0.955 J 0.90 ASSIGNED BY H-H COSY.
Hz ppm Int.2153.56 5.389 37 2147.22 5.373 58 2143.80 5.365 64 2142.70 5.362 100 2142.09 5.360 92 2136.47 5.346 333 2134.64 5.342 96 2132.81 5.337 102 2130.98 5.333 337 2125.37 5.319 83 2124.63 5.317 91 2123.54 5.314 51 2120.24 5.306 51 2113.77 5.290 32 831.91 2.082 30 828.98 2.075 77 828.37 2.073 67 821.41 2.056 238 818.48 2.048 127 815.67 2.041 280 814.21 2.038 358 811.16 2.030 173 808.11 2.023 310 800.66 2.004 133 548.10 1.372 32 545.65 1.366 40 543.95 1.362 55 541.38 1.355 70 537.84 1.346 186 535.64 1.341 186 533.94 1.337 256 532.10 1.332 259 530.64 1.328 536 527.10 1.319 345 523.44 1.310 311 520.14 1.302 118 518.55 1.298 88 517.46 1.295 70 516.97 1.294 68 515.14 1.289 55 512.94 1.284 35 388.79 0.973 524 386.35 0.967 77 381.35 0.955 1000 377.69 0.946 88 376.34 0.942 94 373.78 0.936 545 370.24 0.927 107 368.53 0.923 105 367.19 0.919 116 365.72 0.916 287 363.40 0.910 177 362.55 0.908 188 360.35 0.902 264 358.64 0.898 670 356.57 0.893 189 355.22 0.889 190 354.49 0.888 163 353.64 0.885 169 351.44 0.880 208 349.00 0.874 70 347.66 0.870 52 345.34 0.865 34
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1H NMR 89.56 MHz C8 H16 0.04 ml : 0.5 ml CDCl3 cis-3-octene Assign. Shift(ppm)
A *1 5.35 B *1 5.32 C 2.07 D 1.97 E 1.36 F 1.26 G 0.95 J 0.90
Hz ppm Int.483.75 5.402 129 483.38 5.398 142 481.69 5.379 120 479.88 5.359 99 478.06 5.338 374 476.00 5.315 96 474.31 5.297 128 472.44 5.276 156 197.25 2.203 36 196.50 2.195 37 192.38 2.149 44 190.75 2.130 75 189.63 2.118 111 189.19 2.113 119 187.75 2.097 75 186.81 2.086 76 186.13 2.079 91 184.00 2.055 191 183.19 2.046 172 182.38 2.037 186 181.75 2.030 178 181.38 2.026 171 179.44 2.004 151 178.69 1.996 140 177.88 1.987 130 177.31 1.980 149 176.63 1.973 157 176.06 1.966 159 174.75 1.952 93 173.88 1.942 95 172.94 1.931 73 172.19 1.923 75 171.56 1.916 65 169.75 1.896 49 169.06 1.888 60 168.75 1.885 58 130.19 1.454 30 127.94 1.429 71 124.81 1.394 154 123.75 1.382 170 122.38 1.367 124 121.63 1.359 153 120.63 1.347 241 119.25 1.332 150 118.19 1.320 234 117.00 1.307 253 116.50 1.301 253 115.69 1.292 169 114.63 1.280 148 113.06 1.263 172 111.44 1.245 93 110.13 1.230 129 108.50 1.212 49 107.88 1.205 44 106.69 1.192 42 98.50 1.100 31 93.13 1.040 301 92.63 1.035 404 89.44 0.999 39 87.63 0.979 140 86.50 0.966 242 85.38 0.954 1000 83.63 0.934 165 82.94 0.927 147 81.94 0.915 156 80.25 0.897 468 78.19 0.874 292 77.63 0.867 347 77.00 0.860 241 75.44 0.843 100 74.88 0.837 98 74.25 0.830 109 72.81 0.813 104 72.31 0.808 70 71.31 0.797 49 70.19 0.784 50
in CDCl3
liquid film
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