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网站主页CAS数据库列表 14850-22-7更多图谱顺-3-辛烯(14850-22-7)核磁图(13CNMR)

顺-3-辛烯

产品名称 顺-3-辛烯

CAS号14850-22-7

分子式C8H16

分子量112.21

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  • Mass

    MS-NW-3494          
    cis-3-octene
    C8H16               (Mass of molecular ion:    112)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.6
          26.0       1.9
          27.0      25.0
          28.0       3.9
          29.0      18.8
          38.0       1.9
          39.0      26.0
          40.0       5.0
          41.0     100.0
          42.0      37.5
          43.0      17.7
          50.0       2.0
          51.0       3.7
          52.0       1.8
          53.0      11.1
          54.0       7.5
          55.0      95.4
          56.0      53.5
          57.0      16.4
          58.0       1.2
          63.0       1.1
          65.0       2.3
          66.0       1.1
          67.0      10.3
          68.0       6.6
          69.0      47.1
          70.0      48.4
          71.0       6.4
          77.0       1.6
          79.0       1.7
          81.0       2.7
          82.0       2.0
          83.0      24.1
          84.0       7.4
          85.0       1.5
          97.0       1.9
         112.0      35.8
         113.0       3.4
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H16 0.05 ml : 0.5 ml CDCl3
    cis-3-octene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 5.35 B *1 5.32 C 2.05 D 2.02 E 1.34 F 1.31 G 0.955 J 0.90 ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       2153.56   5.389     37
       2147.22   5.373     58
       2143.80   5.365     64
       2142.70   5.362    100
       2142.09   5.360     92
       2136.47   5.346    333
       2134.64   5.342     96
       2132.81   5.337    102
       2130.98   5.333    337
       2125.37   5.319     83
       2124.63   5.317     91
       2123.54   5.314     51
       2120.24   5.306     51
       2113.77   5.290     32
        831.91   2.082     30
        828.98   2.075     77
        828.37   2.073     67
        821.41   2.056    238
        818.48   2.048    127
        815.67   2.041    280
        814.21   2.038    358
        811.16   2.030    173
        808.11   2.023    310
        800.66   2.004    133
        548.10   1.372     32
        545.65   1.366     40
        543.95   1.362     55
        541.38   1.355     70
        537.84   1.346    186
        535.64   1.341    186
        533.94   1.337    256
        532.10   1.332    259
        530.64   1.328    536
        527.10   1.319    345
        523.44   1.310    311
        520.14   1.302    118
        518.55   1.298     88
        517.46   1.295     70
        516.97   1.294     68
        515.14   1.289     55
        512.94   1.284     35
        388.79   0.973    524
        386.35   0.967     77
        381.35   0.955   1000
        377.69   0.946     88
        376.34   0.942     94
        373.78   0.936    545
        370.24   0.927    107
        368.53   0.923    105
        367.19   0.919    116
        365.72   0.916    287
        363.40   0.910    177
        362.55   0.908    188
        360.35   0.902    264
        358.64   0.898    670
        356.57   0.893    189
        355.22   0.889    190
        354.49   0.888    163
        353.64   0.885    169
        351.44   0.880    208
        349.00   0.874     70
        347.66   0.870     52
        345.34   0.865     34
    


  • 1H NMR 89.56 MHz
    C8 H16 0.04 ml : 0.5 ml CDCl3
    cis-3-octene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 5.35 B *1 5.32 C 2.07 D 1.97 E 1.36 F 1.26 G 0.95 J 0.90

         Hz     ppm     Int.
    

        483.75   5.402    129
        483.38   5.398    142
        481.69   5.379    120
        479.88   5.359     99
        478.06   5.338    374
        476.00   5.315     96
        474.31   5.297    128
        472.44   5.276    156
        197.25   2.203     36
        196.50   2.195     37
        192.38   2.149     44
        190.75   2.130     75
        189.63   2.118    111
        189.19   2.113    119
        187.75   2.097     75
        186.81   2.086     76
        186.13   2.079     91
        184.00   2.055    191
        183.19   2.046    172
        182.38   2.037    186
        181.75   2.030    178
        181.38   2.026    171
        179.44   2.004    151
        178.69   1.996    140
        177.88   1.987    130
        177.31   1.980    149
        176.63   1.973    157
        176.06   1.966    159
        174.75   1.952     93
        173.88   1.942     95
        172.94   1.931     73
        172.19   1.923     75
        171.56   1.916     65
        169.75   1.896     49
        169.06   1.888     60
        168.75   1.885     58
        130.19   1.454     30
        127.94   1.429     71
        124.81   1.394    154
        123.75   1.382    170
        122.38   1.367    124
        121.63   1.359    153
        120.63   1.347    241
        119.25   1.332    150
        118.19   1.320    234
        117.00   1.307    253
        116.50   1.301    253
        115.69   1.292    169
        114.63   1.280    148
        113.06   1.263    172
        111.44   1.245     93
        110.13   1.230    129
        108.50   1.212     49
        107.88   1.205     44
        106.69   1.192     42
         98.50   1.100     31
         93.13   1.040    301
         92.63   1.035    404
         89.44   0.999     39
         87.63   0.979    140
         86.50   0.966    242
         85.38   0.954   1000
         83.63   0.934    165
         82.94   0.927    147
         81.94   0.915    156
         80.25   0.897    468
         78.19   0.874    292
         77.63   0.867    347
         77.00   0.860    241
         75.44   0.843    100
         74.88   0.837     98
         74.25   0.830    109
         72.81   0.813    104
         72.31   0.808     70
         71.31   0.797     49
         70.19   0.784     50
    

in CDCl3



liquid film